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Technology Process of [Co(C5H5N)(ONCC6H5CC6H5NOH)2](CH2C6H3Br)2H

[Co(C5H5N)(ONCC6H5CC6H5NOH)2](CH2C6H3Br)2H

Base Information
  • Chemical Name:[Co(C5H5N)(ONCC6H5CC6H5NOH)2](CH2C6H3Br)2H
  • CAS No.:1009818-66-9
  • Molecular Formula:C47H38Br2CoN5O4
  • Molecular Weight:955.651
  • Hs Code.:
[Co(C<sub>5</sub>H<sub>5</sub>N)(ONCC<sub>6</sub>H<sub>5</sub>CC<sub>6</sub>H<sub>5</sub>NOH)2](CH<sub>2</sub>C<sub>6</sub>H<sub>3</sub>Br)2H

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Chemical Property of [Co(C5H5N)(ONCC6H5CC6H5NOH)2](CH2C6H3Br)2H
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Technology Process of [Co(C5H5N)(ONCC6H5CC6H5NOH)2](CH2C6H3Br)2H

There total 1 articles about [Co(C5H5N)(ONCC6H5CC6H5NOH)2](CH2C6H3Br)2H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro bis(diphenylglyoximato)-pyridinato cobalt

chloro bis(diphenylglyoximato)-pyridinato cobalt

4,4'-dibromo-2,2'-bis(bromomethyl)-1,1'-biphenyl
142068-86-8

4,4'-dibromo-2,2'-bis(bromomethyl)-1,1'-biphenyl

[Co(C<sub>5</sub>H<sub>5</sub>N)(ONCC<sub>6</sub>H<sub>5</sub>CC<sub>6</sub>H<sub>5</sub>NOH)2](CH<sub>2</sub>C<sub>6</sub>H<sub>3</sub>Br)2H
1009818-66-9

[Co(C5H5N)(ONCC6H5CC6H5NOH)2](CH2C6H3Br)2H

[Co(C<sub>5</sub>H<sub>5</sub>N)(ONCC<sub>6</sub>H<sub>5</sub>CC<sub>6</sub>H<sub>5</sub>NOH)2]2(CH<sub>2</sub>C<sub>6</sub>H<sub>3</sub>Br)2

[Co(C5H5N)(ONCC6H5CC6H5NOH)2]2(CH2C6H3Br)2

Guidance literature:
With NaOH; NaBH4; In methanol; diethyl ether; water; aq. soln. of NaOH added to suspn. of Co-complex in MeOH, purged with Ar for 20 min, cooled to 0°C, aq. soln. of NaBH4 added dropwise, soln. of ligand in Et2O added dropwise, stirred in dark for 2-3 h, soln. poured in ice-cold H2O with pyridine; ppt. filtered, washed with H2O, dried over P2O5 in dark, dissolved in CH2Cl2, silica gel column chromy. eluted with ethyl acetate/CH2Cl2 (2-4 %), then with ethyl acetate/CH2Cl2 (10:90);
DOI:10.1021/om7009045
upstream raw materials:

4,4'-dibromo-2,2'-bis(bromomethyl)-1,1'-biphenyl

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