C₂₃H₃₂N₄O₁₅S₂

Base Information

• Chemical Name: C₂₃H₃₂N₄O₁₅S₂
• CAS No.: 857529-43-2
• Molecular Formula: C₂₃H₃₂N₄O₁₅S₂
• Molecular Weight: 668.657
• Mol file: 857529-43-2.mol

Synonyms:

Chemical Property of C₂₃H₃₂N₄O₁₅S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₂N₄O₁₅S₂

There total 5 articles about C₂₃H₃₂N₄O₁₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H32N4O9 → C23H32N4O15S2 (857529-43-2)

Guidance literature:

With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 60 ℃;

DOI:10.1002/cmdc.201200151

Reference yield:

methyl 6-azido-6-deoxy-α-D-mannopyranoside (66224-56-4) → C23H32N4O15S2 (857529-43-2)

Guidance literature:

Multi-step reaction with 5 steps

1.1: CSA / 3 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C

2.2: 6 h / 20 °C

3.1: water; toluene-4-sulfonic acid / methanol; acetonitrile / 3 h / 40 °C

4.1: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 18 h / 20 °C

5.1: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 60 °C

With water; sulfur trioxide trimethylamine complex; sodium hydride; toluene-4-sulfonic acid; copper(II) sulfate; sodium L-ascorbate; In methanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; tert-butyl alcohol; 4.1: Huisgen azide-alkyne cycloaddition;

DOI:10.1002/cmdc.201200151

Reference yield:

methyl 4-O-allyl-6-azido-6-deoxy-2,3-di-O-isopropylidene-α-D-mannopyranoside (857466-25-2) → C23H32N4O15S2 (857529-43-2)

Guidance literature:

Multi-step reaction with 3 steps

1: water; toluene-4-sulfonic acid / methanol; acetonitrile / 3 h / 40 °C

2: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 18 h / 20 °C

3: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 60 °C

With water; sulfur trioxide trimethylamine complex; toluene-4-sulfonic acid; copper(II) sulfate; sodium L-ascorbate; In methanol; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 2: Huisgen azide-alkyne cycloaddition;

DOI:10.1002/cmdc.201200151

upstream raw materials:

methyl 4-O-allyl-6-azido-6-deoxy-2,3-di-O-isopropylidene-α-D-mannopyranoside

methyl 6-azido-6-deoxy-α-D-mannopyranoside

3,4,5-trimethoxy-N-(prop-2-yn-1-yl)benzamide