C₁₇H₂₀N₂O

Base Information

Chemical Name:C₁₇H₂₀N₂O
CAS No.:1368806-98-7
Molecular Formula:C₁₇H₂₀N₂O
Molecular Weight:268.359
Hs Code.:

C<sub>17</sub>H<sub>20</sub>N<sub>2</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₂₀N₂O

Chemical Property:

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Technology Process of C₁₇H₂₀N₂O

There total 5 articles about C₁₇H₂₀N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1368806-97-6
tert-butyl 7-(3-methyl-5-phenylisoxazol-4-yl)hept-6-ynylcarbamate

: 1368806-98-7
C₁₇H₂₀N₂O

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1002/cmdc.201100522

Reference yield:

: 4-phenylbut-3-yn-2-one O-methyl oxime

: 1368806-98-7
C₁₇H₂₀N₂O

Guidance literature:: Multi-step reaction with 3 steps

1: Iodine monochloride / dichloromethane / 20 °C

2: copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 130 °C / Microwave irradiation

3: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

With copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; Iodine monochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; 2: Sonogashira coupling;
DOI:10.1002/cmdc.201100522

Reference yield:

: 16114-53-7
4-iodo-3-methyl-5-phenylisoxazole

: 1368806-98-7
C₁₇H₂₀N₂O

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 130 °C / Microwave irradiation

2: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

With copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; 1: Sonogashira coupling;
DOI:10.1002/cmdc.201100522