4-chloro-N-(4-cyano-3-nitrobenzyl)-2-hydroxylbenzamide

Base Information

Chemical Name:4-chloro-N-(4-cyano-3-nitrobenzyl)-2-hydroxylbenzamide
CAS No.:1333470-06-6
Molecular Formula:C₁₅H₁₀ClN₃O₄
Molecular Weight:331.715
Hs Code.:

Synonyms:

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Chemical Property of 4-chloro-N-(4-cyano-3-nitrobenzyl)-2-hydroxylbenzamide

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Technology Process of 4-chloro-N-(4-cyano-3-nitrobenzyl)-2-hydroxylbenzamide

There total 3 articles about 4-chloro-N-(4-cyano-3-nitrobenzyl)-2-hydroxylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5106-98-9
4-chlorosalicylic acid

: 4-cyano-3-nitrobenzylamine

: 1333470-06-6
4-chloro-N-(4-cyano-3-nitrobenzyl)-2-hydroxylbenzamide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/bi200930f

Reference yield:

: 1333470-04-4
4-(azidomethyl)-2-nitrobenzonitrile

: 1333470-06-6
4-chloro-N-(4-cyano-3-nitrobenzyl)-2-hydroxylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine / tetrahydrofuran; water / 20 °C / Inert atmosphere

2: benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C / Inert atmosphere

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; water;
DOI:10.1021/bi200930f

Reference yield:

: 26830-95-5
4-methyl-2-nitrobenzonitrile

: 1333470-06-6
4-chloro-N-(4-cyano-3-nitrobenzyl)-2-hydroxylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 80 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

3: triphenylphosphine / tetrahydrofuran; water / 20 °C / Inert atmosphere

4: benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C / Inert atmosphere

With N-Bromosuccinimide; sodium azide; 2,2'-azobis(isobutyronitrile); benzotriazol-1-ol; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/bi200930f