C₁₈H₂₂NOP

Base Information

• Chemical Name: C₁₈H₂₂NOP
• CAS No.: 1251472-10-2
• Molecular Formula: C₁₈H₂₂NOP
• Molecular Weight: 299.353
• Mol file: 1251472-10-2.mol

Synonyms:

Chemical Property of C₁₈H₂₂NOP

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₈H₂₂NOP

There total 1 articles about C₁₈H₂₂NOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-pentan-3-one oxime (56134-20-4) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → C18H22NOP (1251472-10-2)

Guidance literature:

2-methyl-pentan-3-one oxime; With triethylamine; In hexane; dichloromethane; at -45 ℃; Inert atmosphere;

chloro-diphenylphosphine; In hexanes; dichloromethane; at -45 - 20 ℃;

DOI:10.1002/chem.201001164

Reference yield:

C18H22NOP (1251472-10-2) → C18H24NOP + C18H24NOP (701292-00-4)

Guidance literature:

With C₄₆H₄₇Cl₂N₃O₄PRe; Dimethylphenylsilane; In dichloromethane; at 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1002/chem.201001164

upstream raw materials:

2-methyl-pentan-3-one oxime

chloro-diphenylphosphine

Downstream raw materials:

C₁₈H₂₄NOP

Refernces