Kemp's triacid L-prolyl amide

Base Information

• Chemical Name: Kemp's triacid L-prolyl amide
• CAS No.: 755002-27-8
• Molecular Formula: C₁₇H₂₅NO₇
• Molecular Weight: 355.388

Synonyms:

Chemical Property of Kemp's triacid L-prolyl amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Kemp's triacid L-prolyl amide

There total 2 articles about Kemp's triacid L-prolyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-1-((1R,5S,7R)-1,5,7-Trimethyl-2,4-dioxo-3-oxa-bicyclo[3.3.1]nonane-7-carbonyl)-pyrrolidine-2-carboxylic acid benzyl ester → Kemp's triacid L-prolyl amide (755002-27-8)

Guidance literature:

With borax; potassium deuteroxide; sodium tetraborate; water-d2; In [D₃]acetonitrile; at 20 ℃;

DOI:10.1016/j.bmcl.2004.06.024

Reference yield:

H-Pro-OBzl (41324-66-7) → Kemp's triacid L-prolyl amide (755002-27-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / pyridine / acetonitrile / 12 h / 20 °C

2: sodium tetraborate; D₂O; KOD / CD₃CN / 20 °C

With pyridine; borax; potassium deuteroxide; sodium tetraborate; water-d2; In [D₃]acetonitrile; acetonitrile;

DOI:10.1016/j.bmcl.2004.06.024

Reference yield:

Kemp's triacid L-prolyl amide (755002-27-8) → Kemp's triacid (79410-20-1)

Guidance literature:

With diclazuril; water-d2; In [D₃]acetonitrile; at 20 ℃; Further Variations:; pD-values; Kinetics;

DOI:10.1016/j.bmcl.2004.06.024

upstream raw materials:

H-Pro-OBzl

Downstream raw materials:

Kemp's triacid

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