Technology Process of C17H26N4O4
There total 9 articles about C17H26N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
1,4-dioxane; methanol;
at 0 - 20 ℃;
for 5h;
DOI:10.1002/cbic.201000177
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1-hydroxy-7-aza-benzotriazole; triethylamine; HATU / dichloromethane / 5 h / 0 - 20 °C
2: palladium on carbon; hydrogen / methanol / 24 h / 20 °C
3: 1-hydroxy-7-aza-benzotriazole; triethylamine; HATU / dichloromethane / 3.5 h / 0 - 20 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C
5: hydrogenchloride / 1,4-dioxane; methanol / 5 h / 0 - 20 °C
With
hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium on carbon; tetrabutyl ammonium fluoride; hydrogen; triethylamine; HATU;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1002/cbic.201000177
- Guidance literature:
-
Multi-step reaction with 6 steps
1: Rh/C; hydrogen; acetic acid / methanol / 24 h / 110 °C / 82745.9 Torr
2: 1-hydroxy-7-aza-benzotriazole; triethylamine; HATU / dichloromethane / 5 h / 0 - 20 °C
3: palladium on carbon; hydrogen / methanol / 24 h / 20 °C
4: 1-hydroxy-7-aza-benzotriazole; triethylamine; HATU / dichloromethane / 3.5 h / 0 - 20 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C
6: hydrogenchloride / 1,4-dioxane; methanol / 5 h / 0 - 20 °C
With
hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; Rh/C; palladium on carbon; tetrabutyl ammonium fluoride; hydrogen; acetic acid; triethylamine; HATU;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1002/cbic.201000177