5'-fluoro-5'-deoxy-2',3'-di-O-acetyl-1-(2,4-dinitrophenyl)inosine

Base Information

Chemical Name:5'-fluoro-5'-deoxy-2',3'-di-O-acetyl-1-(2,4-dinitrophenyl)inosine
CAS No.:1421517-77-2
Molecular Formula:C₂₀H₁₇FN₆O₁₀
Molecular Weight:520.388
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-fluoro-5'-deoxy-2',3'-di-O-acetyl-1-(2,4-dinitrophenyl)inosine

Chemical Property:

Purity/Quality:

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Technology Process of 5'-fluoro-5'-deoxy-2',3'-di-O-acetyl-1-(2,4-dinitrophenyl)inosine

There total 5 articles about 5'-fluoro-5'-deoxy-2',3'-di-O-acetyl-1-(2,4-dinitrophenyl)inosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421517-76-1
5'-fluoro-5'-deoxy-2',3'-di-O-acetylinosine

: 97-00-7
1-chloro-2,4-dinitro-benzene

: 1421517-77-2
5'-fluoro-5'-deoxy-2',3'-di-O-acetyl-1-(2,4-dinitrophenyl)inosine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.3390/molecules171113036

Reference yield:

: 5'-fluoro-5'-deoxy-2',3'-O-isopropylidene-inosine

: 1421517-77-2
5'-fluoro-5'-deoxy-2',3'-di-O-acetyl-1-(2,4-dinitrophenyl)inosine

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / 0 - 20 °C

2: pyridine / 1 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

With pyridine; potassium carbonate; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.3390/molecules171113036

Reference yield:

: 2004-06-0
6-Chloropurine riboside

: 1421517-77-2
5'-fluoro-5'-deoxy-2',3'-di-O-acetyl-1-(2,4-dinitrophenyl)inosine

Guidance literature:: Multi-step reaction with 6 steps

1: toluene-4-sulfonic acid / acetone / 2 h / 20 °C

2: tetrabutyl ammonium fluoride; p-toluenesulfonyl fluoride / tetrahydrofuran / 18 h / Reflux

3: sodium hydroxide / 1,4-dioxane / 4 h / 20 °C

4: trifluoroacetic acid / 0 - 20 °C

5: pyridine / 1 h / 20 °C

6: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

With pyridine; p-toluenesulfonyl fluoride; tetrabutyl ammonium fluoride; potassium carbonate; toluene-4-sulfonic acid; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; acetone;
DOI:10.3390/molecules171113036