C₃₅H₂₂N₄

Base Information

• Chemical Name: C₃₅H₂₂N₄
• CAS No.: 1416070-66-0
• Molecular Formula: C₃₅H₂₂N₄
• Molecular Weight: 498.586
• Mol file: 1416070-66-0.mol

Synonyms:

Chemical Property of C₃₅H₂₂N₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₂₂N₄

There total 2 articles about C₃₅H₂₂N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-amino-6-bromopyrene (42882-08-6) → C35H22N4 (1416070-66-0)

Guidance literature:

Multi-step reaction with 3 steps

1: nitrobenzene; sulfuric acid / 10 h / 110 °C

2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 10 h

3: sodium hydroxide / tetrahydrofuran / 10 h / 80 °C

With sulfuric acid; potassium acetate; nitrobenzene; sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

C19H10BrN (1416070-52-4) → C35H22N4 (1416070-66-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 10 h

2: sodium hydroxide / tetrahydrofuran / 10 h / 80 °C

With potassium acetate; sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; N,N-dimethyl-formamide;

upstream raw materials:

1-amino-6-bromopyrene

C₁₉H₁₀BrN

Refernces