C₄H₂O(Sn(C₄H₉)3)(C(OH)(C₆H₅)2)

Base Information

• Chemical Name: C₄H₂O(Sn(C₄H₉)3)(C(OH)(C₆H₅)2)
• CAS No.: 146300-15-4
• Molecular Formula: C₂₉H₄₀O₂Sn
• Molecular Weight: 539.345
• Mol file: 146300-15-4.mol

Synonyms:

Chemical Property of C₄H₂O(Sn(C₄H₉)3)(C(OH)(C₆H₅)2)

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of C₄H₂O(Sn(C₄H₉)3)(C(OH)(C₆H₅)2)

There total 1 articles about C₄H₂O(Sn(C₄H₉)3)(C(OH)(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

3,4-bis(tri-n-butylstannyl)furan (141700-76-7) → C4H2O(Sn(C4H9)3)(C(OH)(C6H5)2) (146300-15-4)

Guidance literature:

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; n-butyllithium; benzophenone; In tetrahydrofuran; addn. of n-BuLi to soln. of the furan at -78°C, mixt. stirred for 0.5 h, addn. of the electrophile and the pyrimidinone to the lithiated intermediate; react. quenched with saturated NH4Cl, extn. with Et2O, chromy. on neutral alumina;

DOI:10.1039/c39920001723

upstream raw materials:

3,4-bis(tri-n-butylstannyl)furan

Refernces