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Technology Process of C8H13NO

C8H13NO

Base Information
  • Chemical Name:C8H13NO
  • CAS No.:4736-15-6
  • Molecular Formula:C8H13NO
  • Molecular Weight:139.197
  • Hs Code.:
C<sub>8</sub>H<sub>13</sub>NO

Synonyms:

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Chemical Property of C8H13NO
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Technology Process of C8H13NO

There total 1 articles about C8H13NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-cyclohex-3-enecarbaldehyde
7560-64-7

4-methyl-cyclohex-3-enecarbaldehyde

C<sub>8</sub>H<sub>13</sub>NO
4736-15-6

C8H13NO

Guidance literature:
With hydroxylamine; In ethanol; at 20 ℃;
DOI:10.1016/j.tetlet.2011.10.123

Reference yield:

C<sub>8</sub>H<sub>13</sub>NO
4736-15-6

C8H13NO

C<sub>16</sub>H<sub>21</sub>NO

C16H21NO

Guidance literature:
Multi-step reaction with 3 steps
1: trichlorophosphate / dichloromethane / Reflux
2: lithium aluminium tetrahydride / 1,4-dioxane / 3 h / Reflux
3: benzene / 0.5 h / Reflux
With lithium aluminium tetrahydride; trichlorophosphate; In 1,4-dioxane; dichloromethane; benzene;
DOI:10.1016/j.tetlet.2011.10.123

Reference yield:

C<sub>8</sub>H<sub>13</sub>NO
4736-15-6

C8H13NO

C<sub>15</sub>H<sub>18</sub>FN*ClH

C15H18FN*ClH

Guidance literature:
Multi-step reaction with 4 steps
1: trichlorophosphate / dichloromethane / Reflux
2: lithium aluminium tetrahydride / 1,4-dioxane / 3 h / Reflux
3: benzene / 0.5 h / Reflux
4: boron trifluoride diethyl etherate / 1,4-dioxane / 1 h / 180 °C / Microwave irradiation
With lithium aluminium tetrahydride; boron trifluoride diethyl etherate; trichlorophosphate; In 1,4-dioxane; dichloromethane; benzene; 4: aza-Prins reaction;
DOI:10.1016/j.tetlet.2011.10.123
upstream raw materials:

4-methyl-cyclohex-3-enecarbaldehyde

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