C₄₈H₅₀O₁₁SSi

Base Information

Chemical Name:C₄₈H₅₀O₁₁SSi
CAS No.:1315508-24-7
Molecular Formula:C₄₈H₅₀O₁₁SSi
Molecular Weight:863.07
Hs Code.:

C<sub>48</sub>H<sub>50</sub>O<sub>11</sub>SSi

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₅₀O₁₁SSi

Chemical Property:

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Technology Process of C₄₈H₅₀O₁₁SSi

There total 15 articles about C₄₈H₅₀O₁₁SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₈O₇

: 1315508-24-7
C₄₈H₅₀O₁₁SSi

Guidance literature:: Multi-step reaction with 14 steps

1: potassium carbonate / N,N-dimethyl-formamide / 120 h

2: potassium carbonate / N,N-dimethyl-formamide / 22 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Cooling with ice

4: Dess-Martin periodane / dichloromethane / 1.1 h / Cooling with ice

5: ammonium acetate / 13 h / 120 °C

6: sodium tetrahydroborate / methanol; dichloromethane / 0.25 h / Cooling with ice

7: phenyl isocyanate; triethylamine / benzene / 40 h / 45 - 50 °C

8: hydrogen; boric acid / tetrahydrofuran; methanol; water / 21 h

9: 1H-imidazole; triethylamine / dichloromethane / 21 h / Inert atmosphere; Darkness

10: selenium(IV) oxide; water; triethylamine / tetrahydrofuran / 3 h / 50 - 60 °C

11: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h

12: toluene-4-sulfonic acid / benzene / 1 h / 100 - 105 °C

13: boron trifluoride diethyl etherate / dichloromethane / 48 h / 20 °C / Cooling with ice

14: hydrogen; boric acid / tetrahydrofuran; methanol; water / 25 h

With 1H-imidazole; selenium(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; palladium 10% on activated carbon; boron trifluoride diethyl etherate; ammonium acetate; water; hydrogen; boric acid; potassium carbonate; Dess-Martin periodane; phenyl isocyanate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo200399z

Reference yield:

: 1012037-70-5
ethyl 3,4-dihydro-5,6,8-trimethoxy-3,4-dioxonaphthalene-2-carboxylate

: 1315508-24-7
C₄₈H₅₀O₁₁SSi

Guidance literature:: Multi-step reaction with 15 steps

1: sodium dithionite; water / benzene / 0.08 h

2: potassium carbonate / N,N-dimethyl-formamide / 120 h

3: potassium carbonate / N,N-dimethyl-formamide / 22 h / 20 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Cooling with ice

5: Dess-Martin periodane / dichloromethane / 1.1 h / Cooling with ice

6: ammonium acetate / 13 h / 120 °C

7: sodium tetrahydroborate / methanol; dichloromethane / 0.25 h / Cooling with ice

8: phenyl isocyanate; triethylamine / benzene / 40 h / 45 - 50 °C

9: hydrogen; boric acid / tetrahydrofuran; methanol; water / 21 h

10: 1H-imidazole; triethylamine / dichloromethane / 21 h / Inert atmosphere; Darkness

11: selenium(IV) oxide; water; triethylamine / tetrahydrofuran / 3 h / 50 - 60 °C

12: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h

13: toluene-4-sulfonic acid / benzene / 1 h / 100 - 105 °C

14: boron trifluoride diethyl etherate / dichloromethane / 48 h / 20 °C / Cooling with ice

15: hydrogen; boric acid / tetrahydrofuran; methanol; water / 25 h

With 1H-imidazole; selenium(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium dithionite; palladium 10% on activated carbon; boron trifluoride diethyl etherate; ammonium acetate; water; hydrogen; boric acid; potassium carbonate; Dess-Martin periodane; phenyl isocyanate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo200399z

Reference yield:

: 1012037-71-6
3-benzyloxy-4-hydroxy-5,6,8-trimethoxynaphthalene-2-carboxylic acid ethyl ester

: 1315508-24-7
C₄₈H₅₀O₁₁SSi

Guidance literature:: Multi-step reaction with 13 steps

1: potassium carbonate / N,N-dimethyl-formamide / 22 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Cooling with ice

3: Dess-Martin periodane / dichloromethane / 1.1 h / Cooling with ice

4: ammonium acetate / 13 h / 120 °C

5: sodium tetrahydroborate / methanol; dichloromethane / 0.25 h / Cooling with ice

6: phenyl isocyanate; triethylamine / benzene / 40 h / 45 - 50 °C

7: hydrogen; boric acid / tetrahydrofuran; methanol; water / 21 h

8: 1H-imidazole; triethylamine / dichloromethane / 21 h / Inert atmosphere; Darkness

9: selenium(IV) oxide; water; triethylamine / tetrahydrofuran / 3 h / 50 - 60 °C

10: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h

11: toluene-4-sulfonic acid / benzene / 1 h / 100 - 105 °C

12: boron trifluoride diethyl etherate / dichloromethane / 48 h / 20 °C / Cooling with ice

13: hydrogen; boric acid / tetrahydrofuran; methanol; water / 25 h

With 1H-imidazole; selenium(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; palladium 10% on activated carbon; boron trifluoride diethyl etherate; ammonium acetate; water; hydrogen; boric acid; potassium carbonate; Dess-Martin periodane; phenyl isocyanate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo200399z