Technology Process of C35H46BrN3O7
There total 7 articles about C35H46BrN3O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: palladium on activated charcoal / methanol / 18 h
2.1: AD column / methanol; hexane; isopropyl alcohol / Resolution of racemate
2.2: 18 h
3.1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water
4.1: chloroamine-T / methanol / 0.33 h
5.1: 3 h / 60 °C
With
palladium on activated charcoal; hydroxylamine hydrochloride; chloroamine-T; sodium carbonate;
In
methanol; ethanol; hexane; water; isopropyl alcohol;
DOI:10.1016/j.bmcl.2012.03.014
- Guidance literature:
-
Multi-step reaction with 2 steps
1: chloroamine-T / methanol / 0.33 h
2: 3 h / 60 °C
With
chloroamine-T;
In
methanol;
DOI:10.1016/j.bmcl.2012.03.014
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: AD column / methanol; hexane; isopropyl alcohol / Resolution of racemate
1.2: 18 h
2.1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water
3.1: chloroamine-T / methanol / 0.33 h
4.1: 3 h / 60 °C
With
hydroxylamine hydrochloride; chloroamine-T; sodium carbonate;
In
methanol; ethanol; hexane; water; isopropyl alcohol;
DOI:10.1016/j.bmcl.2012.03.014