Technology Process of SF2523
There total 5 articles about SF2523 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); caesium carbonate;
In
1,2-dimethoxyethane;
at 130 ℃;
for 0.25h;
Microwave irradiation;
DOI:10.1021/jm301522m
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / 0 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: trifluoromethylsulfonic anhydride / dichloromethane / 20 °C
3.1: caesium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane / 0.25 h / 130 °C / Microwave irradiation
With
tetrakis(triphenylphosphine) palladium(0); trifluoromethylsulfonic anhydride; caesium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; 1,2-dimethoxyethane; hexane; dichloromethane;
3.1: |Suzuki Coupling;
DOI:10.1021/jm301522m
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / 0 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: trifluoromethylsulfonic anhydride / dichloromethane / 20 °C
3.1: caesium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane / 0.25 h / 130 °C / Microwave irradiation
With
tetrakis(triphenylphosphine) palladium(0); trifluoromethylsulfonic anhydride; caesium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; 1,2-dimethoxyethane; hexane; dichloromethane;
3.1: |Suzuki Coupling;
DOI:10.1021/jm301522m
