C₁₈H₂₃NO

Base Information

• Chemical Name: C₁₈H₂₃NO
• CAS No.: 1549684-57-2
• Molecular Formula: C₁₈H₂₃NO
• Molecular Weight: 269.387
• Mol file: 1549684-57-2.mol

Synonyms:

Chemical Property of C₁₈H₂₃NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₂₃NO

There total 4 articles about C₁₈H₂₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(4'-azidobutyl)-spiro[bicyclo[2.2.1]heptane-2-2'-[1,3]dioxolan]-5-one (450392-90-2) → C18H23NO (1549684-57-2)

Guidance literature:

Multi-step reaction with 5 steps

1: titanium tetrachloride / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

2: chloro-trimethyl-silane / Inert atmosphere

3: Inert atmosphere

4: sodium cyanoborohydride / Inert atmosphere

5: hydrogenchloride / Inert atmosphere

With hydrogenchloride; chloro-trimethyl-silane; titanium tetrachloride; sodium cyanoborohydride; In dichloromethane; 1: |Schmidt Reaction / 3: |Grignard Reaction;

DOI:10.1038/nchem.1844

Reference yield:

C20H27NO3 → C18H23NO (1549684-57-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium cyanoborohydride / Inert atmosphere

2: hydrogenchloride / Inert atmosphere

With hydrogenchloride; sodium cyanoborohydride;

DOI:10.1038/nchem.1844

Reference yield:

7-azatricyclo[7.2.1.0]dodecane-8,11-dione (450392-91-3) → C18H23NO (1549684-57-2)

Guidance literature:

Multi-step reaction with 4 steps

1: chloro-trimethyl-silane / Inert atmosphere

2: Inert atmosphere

3: sodium cyanoborohydride / Inert atmosphere

4: hydrogenchloride / Inert atmosphere

With hydrogenchloride; chloro-trimethyl-silane; sodium cyanoborohydride; 2: |Grignard Reaction;

DOI:10.1038/nchem.1844

upstream raw materials:

6-(4'-azidobutyl)-spiro[bicyclo[2.2.1]heptane-2-2'-[1,3]dioxolan]-5-one

7-azatricyclo[7.2.1.0]dodecane-8,11-dione

Downstream raw materials:

C₁₈H₂₅NO