C₃₈H₅₅NO₃Si

Base Information

Chemical Name:C₃₈H₅₅NO₃Si
CAS No.:1583281-43-9
Molecular Formula:C₃₈H₅₅NO₃Si
Molecular Weight:601.945
Hs Code.:

C<sub>38</sub>H<sub>55</sub>NO<sub>3</sub>Si

Synonyms:

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Chemical Property of C₃₈H₅₅NO₃Si

Chemical Property:

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Technology Process of C₃₈H₅₅NO₃Si

There total 18 articles about C₃₈H₅₅NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1583281-41-7
C₄₀H₅₉NO₃Si

: 1583281-43-9
C₃₈H₅₅NO₃Si

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In toluene; at 60 ℃; Inert atmosphere;
DOI:10.1002/asia.201301248

Reference yield:

: C₁₉H₂₄O₃

: 1583281-43-9
C₃₈H₅₅NO₃Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: mesitylenesulfonylhydroxylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

2.1: ozone / dichloromethane; isopropyl alcohol / 0.17 h / -78 °C / Inert atmosphere

2.2: 0.75 h / -78 - 0 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran / Reflux; Inert atmosphere

4.1: lithium borohydride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

5.1: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere

6.1: ammonium cerium (IV) nitrate / water; acetonitrile / 0 °C / Inert atmosphere

7.1: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 20 °C / Inert atmosphere

8.1: triethylamine; lithium chloride / tetrahydrofuran / 30 °C / Inert atmosphere

9.1: acetic acid; hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / 25 °C

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

11.1: pyridinium p-toluenesulfonate / ethanol / 25 °C / Inert atmosphere

12.1: ortho-nitrophenyl selenocyanate; tributylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

12.2: 20 °C / Inert atmosphere

13.1: sodium tetrahydroborate / ethanol / 20 °C / Inert atmosphere

14.1: potassium carbonate / acetonitrile / 90 °C / Inert atmosphere

15.1: Hoveyda-Grubbs catalyst second generation / toluene / 60 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; lithium borohydride; Hoveyda-Grubbs catalyst second generation; ortho-nitrophenyl selenocyanate; ammonium cerium (IV) nitrate; tributylphosphine; 10 wt% Pd(OH)2 on carbon; hydrogen; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; mesitylenesulfonylhydroxylamine; sodium hydride; potassium carbonate; ozone; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol; toluene; acetonitrile; 2.2: |Clemmensen Reduction / 7.1: |Parikh-Doering Oxidation;
DOI:10.1002/asia.201301248

Reference yield:

: C₁₈H₂₃NO₄

: 1583281-43-9
C₃₈H₅₅NO₃Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: zinc; chloro-trimethyl-silane / water; tetrahydrofuran / 24 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / Reflux; Inert atmosphere

3.1: lithium borohydride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere

5.1: ammonium cerium (IV) nitrate / water; acetonitrile / 0 °C / Inert atmosphere

6.1: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 20 °C / Inert atmosphere

7.1: triethylamine; lithium chloride / tetrahydrofuran / 30 °C / Inert atmosphere

8.1: acetic acid; hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / 25 °C

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

10.1: pyridinium p-toluenesulfonate / ethanol / 25 °C / Inert atmosphere

11.1: ortho-nitrophenyl selenocyanate; tributylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

11.2: 20 °C / Inert atmosphere

12.1: sodium tetrahydroborate / ethanol / 20 °C / Inert atmosphere

13.1: potassium carbonate / acetonitrile / 90 °C / Inert atmosphere

14.1: Hoveyda-Grubbs catalyst second generation / toluene / 60 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; lithium borohydride; chloro-trimethyl-silane; Hoveyda-Grubbs catalyst second generation; ortho-nitrophenyl selenocyanate; ammonium cerium (IV) nitrate; tributylphosphine; 10 wt% Pd(OH)2 on carbon; hydrogen; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; zinc; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; toluene; acetonitrile; 6.1: |Parikh-Doering Oxidation;
DOI:10.1002/asia.201301248