C₂₇H₃₃NO₄SSi

Base Information

Chemical Name:C₂₇H₃₃NO₄SSi
CAS No.:1261034-19-8
Molecular Formula:C₂₇H₃₃NO₄SSi
Molecular Weight:495.715
Hs Code.:

C<sub>27</sub>H<sub>33</sub>NO<sub>4</sub>SSi

Synonyms:

Suppliers and Price of C₂₇H₃₃NO₄SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₃NO₄SSi

Chemical Property:

Purity/Quality:

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Technology Process of C₂₇H₃₃NO₄SSi

There total 1 articles about C₂₇H₃₃NO₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1221741-06-5
(S)-N-(methanesulfonyl)homotyrosinol

: 1261034-19-8
C₂₇H₃₃NO₄SSi

Guidance literature:: Multi-step reaction with 2 steps

1: [bis(acetoxy)iodo]benzene; trifluoroacetic acid / 20 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With 1H-imidazole; [bis(acetoxy)iodo]benzene; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/chem.201001402

Reference yield:

: 1261034-19-8
C₂₇H₃₃NO₄SSi

: 1261033-34-4
C₂₇H₃₇NO₃SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hexamethylsilazane / -100 °C / Inert atmosphere

2.1: 10% palladium on activated carbon; hydrogen / ethanol / 760.05 Torr / Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: nickel dichloride / methanol; ethanol / 0.5 h / Inert atmosphere

4.2: 0 °C / Inert atmosphere

With 10% palladium on activated carbon; boron trifluoride diethyl etherate; hydrogen; potassium hexamethylsilazane; nickel dichloride; In methanol; ethanol; dichloromethane; 1.1: Michael cyclization;
DOI:10.1002/chem.201001402

Reference yield:

: 1261034-19-8
C₂₇H₃₃NO₄SSi

: 1261033-39-9
C₃₅H₅₁NO₄SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hexamethylsilazane / -100 °C / Inert atmosphere

2.1: 10% palladium on activated carbon; hydrogen / ethanol / 760.05 Torr / Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: nickel dichloride / methanol; ethanol / 0.5 h / Inert atmosphere

4.2: 0 °C / Inert atmosphere

5.1: tert.-butyl lithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

5.2: 0.25 h / -78 °C / Inert atmosphere

5.3: 2 h / -78 °C / Inert atmosphere

6.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

With 10% palladium on activated carbon; boron trifluoride diethyl etherate; hydrogen; tert.-butyl lithium; potassium hexamethylsilazane; Dess-Martin periodane; nickel dichloride; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; 1.1: Michael cyclization / 6.1: Dess-Martin oxidation;
DOI:10.1002/chem.201001402