C₃₀H₄₁N₃O₈

Base Information

Chemical Name:C₃₀H₄₁N₃O₈
CAS No.:1255213-03-6
Molecular Formula:C₃₀H₄₁N₃O₈
Molecular Weight:571.671
Hs Code.:

C<sub>30</sub>H<sub>41</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₃₀H₄₁N₃O₈

Chemical Property:

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Technology Process of C₃₀H₄₁N₃O₈

There total 11 articles about C₃₀H₄₁N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₄₂FN₃O₈

: 1255213-03-6
C₃₀H₄₁N₃O₈

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃;
DOI:10.1021/ja105119r

Reference yield:

: 1255212-57-7
(1R,2S)-1-phenyl-2-(N,2,4,6-tetramethylphenylsulfonamido)propyl (2R,3S)-4-(tert-butoxycarbonyl(methyl)amino)-3-hydroxy-2-methylbutanoate

: 1255213-03-6
C₃₀H₄₁N₃O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: water; dihydrogen peroxide; sodium hydroxide / methanol; tert-butyl alcohol / 0 - 20 °C

1.2: pH 4

2.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 65 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

6.1: ammonium fluoride; tetrabutyl ammonium fluoride / tetrahydrofuran / 40 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 20 °C

With 2,6-dimethylpyridine; ammonium fluoride; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; dihydrogen peroxide; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; mineral oil; tert-butyl alcohol;
DOI:10.1021/ja105119r

Reference yield:

: 1255212-61-3
(2R,3S)-4-(tert-butoxycarbonyl(methyl)amino)-3-hydroxy-2-methylbutanoic acid

: 1255213-03-6
C₃₀H₄₁N₃O₈

Guidance literature:: Multi-step reaction with 6 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 65 °C / Inert atmosphere

4: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

5: ammonium fluoride; tetrabutyl ammonium fluoride / tetrahydrofuran / 40 °C

6: sodium hydride / tetrahydrofuran; mineral oil / 20 °C

With 2,6-dimethylpyridine; ammonium fluoride; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ja105119r