diphospha(2,4,6-trimethylbenzene)2diboro((CH₃)2CH(CH₃)2C)

Base Information

Chemical Name:diphospha(2,4,6-trimethylbenzene)2diboro((CH₃)2CH(CH₃)2C)
CAS No.:117229-49-9
Molecular Formula:0C₂H₅O*C₃₀H₄₈B₂P₂
Molecular Weight:522.021
Hs Code.:

diphospha(2,4,6-trimethylbenzene)2diboro((CH<sub>3</sub>)2CH(CH<sub>3</sub>)2C)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphospha(2,4,6-trimethylbenzene)2diboro((CH₃)2CH(CH₃)2C)

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Technology Process of diphospha(2,4,6-trimethylbenzene)2diboro((CH₃)2CH(CH₃)2C)

There total 1 articles about diphospha(2,4,6-trimethylbenzene)2diboro((CH₃)2CH(CH₃)2C) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 89634-37-7,147285-62-9
lithium 2,4,6-trimethylphenylhydrophosphanide

: 79200-82-1
(thexyl)dichloroborane

: 117229-49-9
diphospha(2,4,6-trimethylbenzene)2diboro((CH₃)2CH(CH₃)2C)

Guidance literature:: In diethyl ether; hexane; Under Ar or N2 ThexylBCL2 in hexane is added dropwise to a soln. of MesPHLi in Et2O at 0°C, stirring overnight at room temp.; Volatile is removed under vac., residue is extracted into hexane, filtered, filtrate is concentrated under reduced pressure, Et2O is added, mixt. is cooled at -78°C.;
DOI:10.1021/ja00183a025