tetrachlorobis(salicylaldehyde-N'-2-thiazolyl sulphanilamide)germanate

Base Information

• Chemical Name: tetrachlorobis(salicylaldehyde-N'-2-thiazolyl sulphanilamide)germanate
• CAS No.: 101965-88-2
• Molecular Formula: C₃₂H₂₆Cl₄GeN₆O₆S₄
• Molecular Weight: 933.261
• Mol file: 101965-88-2.mol

Synonyms:

Chemical Property of tetrachlorobis(salicylaldehyde-N'-2-thiazolyl sulphanilamide)germanate

Chemical Property:

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Useful:

Technology Process of tetrachlorobis(salicylaldehyde-N'-2-thiazolyl sulphanilamide)germanate

There total 1 articles about tetrachlorobis(salicylaldehyde-N'-2-thiazolyl sulphanilamide)germanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4‐((2‐hydroxybenzylidene)amino)‐N‐(thiazol‐2‐yl)benzenesulfonamide (7354-98-5) + germaniumtetrachloride (10038-98-9) → tetrachlorobis(salicylaldehyde-N'-2-thiazolyl sulphanilamide)germanate (101965-88-2)

Guidance literature:

In benzene; to a soln. of GeCl4 in benzene the ligand in 1:2 molar ratio was added,the mixt. was stirred for 3-4 h, the product sepd. slowly; the solvent was decanted off, the solid was washed with benzene, the solvent was removed in vac., dried at 40-50°C 0.05 mm for 2-3 h; elem. anal.;

upstream raw materials:

4‐((2‐hydroxybenzylidene)amino)‐N‐(thiazol‐2‐yl)benzenesulfonamide

germaniumtetrachloride