(diphenylphosphinoethyl)diphenylphosphine oxide

Base Information

Chemical Name:(diphenylphosphinoethyl)diphenylphosphine oxide
CAS No.:53849-92-6
Molecular Formula:C₂₆H₂₄OP₂
Molecular Weight:414.423
Hs Code.:

Synonyms:

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Chemical Property of (diphenylphosphinoethyl)diphenylphosphine oxide

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Technology Process of (diphenylphosphinoethyl)diphenylphosphine oxide

There total 1 articles about (diphenylphosphinoethyl)diphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53849-92-6
(diphenylphosphinoethyl)diphenylphosphine oxide

Guidance literature:: Ph3PO, CH3Li;
DOI:10.1021/ic50145a044

Reference yield: 86.0%

: 26042-64-8
silver hexafluoroantimonate

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 53849-92-6
(diphenylphosphinoethyl)diphenylphosphine oxide

: (C₃H₇)C₆H₄CH₃RuClP(C₆H₅)2CHCH₃P(C₆H₅)2O⁽¹⁺⁾*SbF₆^(1-)=CH₃C₆H₄C₃H₇RuClP(C₆H₅)2CHCH₃P(C₆H₅)2O(SbF₆)

Guidance literature:: In dichloromethane; a mixt. of diphosphine and complex in CH2Cl2 was stirred for 10 min, AgBF6 in CH2Cl2 was added, stirred for 12 h (inert atm.); filtered, washed with Ch2Cl2, the filtrates were combined, the solvent was removed in vac., dissolved in CH2Cl2, chromd. on silica gel (EtOAc);
DOI:10.1021/om000319s

Reference yield: 80.4%

: [osmium(II)dichloride(η6-p-cymene)]2

: 53849-92-6
(diphenylphosphinoethyl)diphenylphosphine oxide

: 296766-33-1
[(η6-cymene)OsCl2(η1-(C6H5)2PCH(CH3)P(O)(C6H5)2-P)]

Guidance literature:: In dichloromethane; under N2; to a soln. of the complex in CH2Cl2 was added the ligand, themixt. was stirred at 25°C for 2 h; the solvent was evapd. under vac., ppt. was chromd. (silica gel, CH3CO2CH2CH3/hexanes), the solvent was evapd. under vac., ppt. was recrystd. (CH2Cl2/(CH3CH2)2O); elem. anal.;
DOI:10.1021/om000083s