N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-6-benzyloxycarbonylamino-5-O-triethylsilyl-6-deoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-glycelo-L-talo-heptofuranuronamide

Base Information

Chemical Name:N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-6-benzyloxycarbonylamino-5-O-triethylsilyl-6-deoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-glycelo-L-talo-heptofuranuronamide
CAS No.:1037307-60-0
Molecular Formula:C₃₂H₄₂N₄O₁₂
Molecular Weight:674.705
Hs Code.:

N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-6-benzyloxycarbonylamino-5-O-triethylsilyl-6-deoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-glycelo-L-talo-heptofuranuronamide

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Chemical Property of N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-6-benzyloxycarbonylamino-5-O-triethylsilyl-6-deoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-glycelo-L-talo-heptofuranuronamide

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Technology Process of N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-6-benzyloxycarbonylamino-5-O-triethylsilyl-6-deoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-glycelo-L-talo-heptofuranuronamide

There total 1 articles about N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-6-benzyloxycarbonylamino-5-O-triethylsilyl-6-deoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-glycelo-L-talo-heptofuranuronamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1004751-05-6
tert-butyl (2S,3S)-3-[(tert-butyldiphenylsilyl)oxy]-2-(methylamino)pent-4-enoate

: 1037307-57-5
C₂₈H₃₉N₃O₁₀Si

: 1037307-60-0
N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-6-benzyloxycarbonylamino-5-O-triethylsilyl-6-deoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-glycelo-L-talo-heptofuranuronamide

Guidance literature:: tert-butyl (2S,3S)-3-[(tert-butyldiphenylsilyl)oxy]-2-(methylamino)pent-4-enoate; C₂₈H₃₉N₃O₁₀Si; With sodium hydrogencarbonate; In tetrahydrofuran; at 20 ℃; for 18h;

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 168h; Further stages.;
DOI:10.1016/j.bmc.2008.03.020