C₉H₁₀⁽²⁾HNO₃

Base Information

Chemical Name:C₉H₁₀⁽²⁾HNO₃
CAS No.:73549-13-0
Molecular Formula:C₉H₁₁NO₃
Molecular Weight:182.183
Hs Code.:

C<sub>9</sub>H<sub>10</sub><sup>(2)</sup>HNO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₁₀⁽²⁾HNO₃

Chemical Property:

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Technology Process of C₉H₁₀⁽²⁾HNO₃

There total 4 articles about C₉H₁₀⁽²⁾HNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₄⁽²⁾HNO₄

: 73549-13-0
C₉H₁₀⁽²⁾HNO₃

Guidance literature:: C₁₆H₁₄⁽²⁾HNO₄; With hydrogen bromide; In water; Reflux;

With acetic acid; sodium hydroxide; at 0 ℃;
DOI:10.1021/ja403918w

Reference yield:

: 64896-32-8
(Z)-2-benzamido-3-(p-hydroxyphenyl)-2-propenic acid

: 73549-13-0
C₉H₁₀⁽²⁾HNO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: [Rh(NBD)((R)-Prophos)]ClO₄; deuterium / tetrahydrofuran / 1500.15 Torr

1.2: Dowex 50 W (100?200 mesh) cation exchange resin

2.1: hydrogen bromide / water / Reflux

2.2: 0 °C

With [Rh(NBD)((R)-Prophos)]ClO₄; hydrogen bromide; deuterium; In tetrahydrofuran; water;
DOI:10.1021/ja403918w

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 73549-13-0
C₉H₁₀⁽²⁾HNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: dipotassium hydrogenphosphate; acetic anhydride / 0.08 h / 80 °C / Inert atmosphere

1.2: 2 h / 80 °C / Inert atmosphere

2.1: sodium hydroxide; water / ethanol / 12 h / Reflux

3.1: [Rh(NBD)((R)-Prophos)]ClO₄; deuterium / tetrahydrofuran / 1500.15 Torr

3.2: Dowex 50 W (100?200 mesh) cation exchange resin

4.1: hydrogen bromide / water / Reflux

4.2: 0 °C

With dipotassium hydrogenphosphate; [Rh(NBD)((R)-Prophos)]ClO₄; water; hydrogen bromide; acetic anhydride; deuterium; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/ja403918w