C₂₆H₂₈N₂O₃

Base Information

• Chemical Name: C₂₆H₂₈N₂O₃
• CAS No.: 1435485-68-9
• Molecular Formula: C₂₆H₂₈N₂O₃
• Molecular Weight: 416.52
• Mol file: 1435485-68-9.mol

Synonyms:

Chemical Property of C₂₆H₂₈N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₈N₂O₃

There total 4 articles about C₂₆H₂₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C27H30N2O3 → C26H28N2O3 (1435485-68-9)

Guidance literature:

With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/ml400073g

Reference yield:

1-bromomethyl-3-nitrobenzene (3958-57-4) → C26H28N2O3 (1435485-68-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: triethylamine / acetonitrile / 0 - 20 °C

2.1: palladium 10% on activated carbon / ethanol / 1 h / Inert atmosphere; Reflux

2.2: 2 h / Inert atmosphere; Reflux

3.1: triethylamine / tetrahydrofuran / 3.17 h / 0 - 20 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

With palladium 10% on activated carbon; water; triethylamine; lithium hydroxide; In tetrahydrofuran; ethanol; acetonitrile;

DOI:10.1021/ml400073g

Reference yield:

dibenzylamine (103-49-1) → C26H28N2O3 (1435485-68-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: triethylamine / acetonitrile / 0 - 20 °C

2.1: palladium 10% on activated carbon / ethanol / 1 h / Inert atmosphere; Reflux

2.2: 2 h / Inert atmosphere; Reflux

3.1: triethylamine / tetrahydrofuran / 3.17 h / 0 - 20 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

With palladium 10% on activated carbon; water; triethylamine; lithium hydroxide; In tetrahydrofuran; ethanol; acetonitrile;

DOI:10.1021/ml400073g

upstream raw materials:

1-bromomethyl-3-nitrobenzene

dibenzylamine

N,N-dibenzyl-1-(3-nitrophenyl)methylamine

Downstream raw materials:

C₄₉H₆₂N₁₂O₆

C₆₇H₈₅N₁₅O₉S

Refernces