methyl (S)-3-(3-methoxymethoxy-4-methylphenyl)butanoate

Base Information

Chemical Name:methyl (S)-3-(3-methoxymethoxy-4-methylphenyl)butanoate
CAS No.:151697-19-7
Molecular Formula:C₁₄H₂₀O₄
Molecular Weight:252.31
Hs Code.:

Synonyms:

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Chemical Property of methyl (S)-3-(3-methoxymethoxy-4-methylphenyl)butanoate

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Technology Process of methyl (S)-3-(3-methoxymethoxy-4-methylphenyl)butanoate

There total 7 articles about methyl (S)-3-(3-methoxymethoxy-4-methylphenyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1201-85-0
(S)-3-(4-methylphenyl)butanoic acid

: 151697-19-7
methyl (S)-3-(3-methoxymethoxy-4-methylphenyl)butanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 2.3 g / nitric acid, conc. sulfuric acid, glacial acetic acid / CH₂Cl₂ / 0.25 h / -15 °C

2: 75 percent / diethyl ether / 0.17 h / 0 °C

3: hydrogen / platinum oxide / ethanol / 6.5 h / Ambient temperature

4: 1.) NaNO₂, 5N H₂SO₄, 2.) saturated aq. CuSO₄ / 1.) H₂O, 2.) 90 deg C, 1 h

5: 494 mg / diisopropylethylamine / CH₂Cl₂ / 3 h / 40 °C

With sulfuric acid; hydrogen; nitric acid; copper(II) sulfate; acetic acid; N-ethyl-N,N-diisopropylamine; sodium nitrite; platinum(IV) oxide; In diethyl ether; ethanol; dichloromethane;

Reference yield:

: 151765-65-0
(S)-3-(4-methylphenyl)butanal

: 151697-19-7
methyl (S)-3-(3-methoxymethoxy-4-methylphenyl)butanoate

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / sodium chlorite, sodium dihydrogen phosphate / 2-methyl-propan-2-ol; H₂O; various solvent(s) / Ambient temperature

2: 2.3 g / nitric acid, conc. sulfuric acid, glacial acetic acid / CH₂Cl₂ / 0.25 h / -15 °C

3: 75 percent / diethyl ether / 0.17 h / 0 °C

4: hydrogen / platinum oxide / ethanol / 6.5 h / Ambient temperature

5: 1.) NaNO₂, 5N H₂SO₄, 2.) saturated aq. CuSO₄ / 1.) H₂O, 2.) 90 deg C, 1 h

6: 494 mg / diisopropylethylamine / CH₂Cl₂ / 3 h / 40 °C

With sodium chlorite; sodium dihydrogen phosphate; sulfuric acid; hydrogen; nitric acid; copper(II) sulfate; acetic acid; N-ethyl-N,N-diisopropylamine; sodium nitrite; platinum(IV) oxide; In diethyl ether; ethanol; dichloromethane; water; tert-butyl alcohol;

Reference yield:

: 97372-48-0
(S)-3-(4-Methyl-3-nitro-phenyl)-butyric acid

: 151697-19-7
methyl (S)-3-(3-methoxymethoxy-4-methylphenyl)butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / diethyl ether / 0.17 h / 0 °C

2: hydrogen / platinum oxide / ethanol / 6.5 h / Ambient temperature

3: 1.) NaNO₂, 5N H₂SO₄, 2.) saturated aq. CuSO₄ / 1.) H₂O, 2.) 90 deg C, 1 h

4: 494 mg / diisopropylethylamine / CH₂Cl₂ / 3 h / 40 °C

With sulfuric acid; hydrogen; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; sodium nitrite; platinum(IV) oxide; In diethyl ether; ethanol; dichloromethane;