(S)-2-{(S)-2-[(S)-2-(4-tert-Butoxycarbonylamino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid methyl ester

Base Information

• Chemical Name: (S)-2-{(S)-2-[(S)-2-(4-tert-Butoxycarbonylamino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid methyl ester
• CAS No.: 1026967-39-4
• Molecular Formula: C₃₄H₄₈N₄O₇
• Molecular Weight: 624.778

Synonyms:

Chemical Property of (S)-2-{(S)-2-[(S)-2-(4-tert-Butoxycarbonylamino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid methyl ester

Chemical Property:

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Technology Process of (S)-2-{(S)-2-[(S)-2-(4-tert-Butoxycarbonylamino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid methyl ester

There total 1 articles about (S)-2-{(S)-2-[(S)-2-(4-tert-Butoxycarbonylamino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(tert-butoxycarbonyl)-4-aminobutanoic acid (57294-38-9) + (S)-2-[(S)-2-((S)-2-Amino-3-phenyl-propionylamino)-4-methyl-pentanoylamino]-3-phenyl-propionic acid methyl ester; compound with trifluoro-acetic acid → (S)-2-{(S)-2-[(S)-2-(4-tert-Butoxycarbonylamino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid methyl ester (1026967-39-4)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;

DOI:10.1021/jm00040a001

Reference yield:

(S)-2-{(S)-2-[(S)-2-(4-tert-Butoxycarbonylamino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid methyl ester (1026967-39-4) → (S)-2-{(S)-2-[(S)-2-(4-Amino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid methyl ester

Guidance literature:

With trifluoroacetic acid; at 0 ℃;

DOI:10.1021/jm00040a001

Reference yield:

(S)-2-{(S)-2-[(S)-2-(4-tert-Butoxycarbonylamino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid methyl ester (1026967-39-4) → (3-{(S)-1-[(S)-1-((S)-1-Hydroxymethyl-2-phenyl-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-2-phenyl-ethylcarbamoyl}-propyl)-carbamic acid tert-butyl ester (1026820-99-4)

Guidance literature:

With lithium borohydride; In tetrahydrofuran; methanol;

DOI:10.1021/jm00040a001

upstream raw materials:

N-(tert-butoxycarbonyl)-4-aminobutanoic acid

Downstream raw materials:

(3-{(S)-1-[(S)-1-((S)-1-Hydroxymethyl-2-phenyl-ethylcarbamoyl)-3-methyl-butylcarbamoyl]-2-phenyl-ethylcarbamoyl}-propyl)-carbamic acid tert-butyl ester

(S)-2-[(S)-2-(4-Amino-butyrylamino)-3-phenyl-propionylamino]-4-methyl-pentanoic acid ((S)-1-hydroxymethyl-2-phenyl-ethyl)-amide

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