Technology Process of C32H25P
There total 6 articles about C32H25P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(M)-(3',4'-dihydro-[1,1'-binaphthalen]-2-yl)diphenylphosphine oxide;
With
oxalyl dichloride;
In
dichloromethane;
at 20 ℃;
for 0.5h;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 3.5h;
DOI:10.1002/anie.201509571
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium diacetate; lithium tert-butoxide; C35H32F4NO4P / 1,4-dioxane / 24 h / 50 °C / Schlenk technique; Inert atmosphere
2.1: oxalyl dichloride / dichloromethane / 0.5 h / 20 °C
2.2: 3.5 h / 0 - 20 °C
With
oxalyl dichloride; C35H32F4NO4P; palladium diacetate; lithium tert-butoxide;
In
1,4-dioxane; dichloromethane;
DOI:10.1002/anie.201509571
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium diacetate; lithium tert-butoxide; C35H32F4NO4P / 1,4-dioxane / 24 h / 50 °C / Schlenk technique; Inert atmosphere
2.1: oxalyl dichloride / dichloromethane / 0.5 h / 20 °C
2.2: 3.5 h / 0 - 20 °C
With
oxalyl dichloride; C35H32F4NO4P; palladium diacetate; lithium tert-butoxide;
In
1,4-dioxane; dichloromethane;
DOI:10.1002/anie.201509571