(3,5-Me₂C₆H₃N(1-adamantyl))3NbCl

Base Information

Chemical Name:(3,5-Me₂C₆H₃N(1-adamantyl))3NbCl
CAS No.:215254-46-9
Molecular Formula:C₅₄H₇₂ClN₃Nb
Molecular Weight:891.545
Hs Code.:

(3,5-Me<sub>2</sub>C<sub>6</sub>H<sub>3</sub>N(1-adamantyl))3NbCl

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Chemical Property of (3,5-Me₂C₆H₃N(1-adamantyl))3NbCl

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Technology Process of (3,5-Me₂C₆H₃N(1-adamantyl))3NbCl

There total 1 articles about (3,5-Me₂C₆H₃N(1-adamantyl))3NbCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: NbCl₄(THF)₂

: 215180-13-5
Li⁽¹⁺⁾*N(C₁₀H₁₅)(C₆H₃(CH₃)2)^(1-)*C₄H₁₀O = Li[N(C₁₀H₁₅)(C₆H₃(CH₃)2)]*C₄H₁₀O

: 215254-46-9
(3,5-Me₂C₆H₃N(1-adamantyl))3NbCl

Guidance literature:: In diethyl ether; byproducts: LiCl; inert atmosphere; stirring Nb-complex with 3 equiv. of Li-salt (room temp., 8 h, pptn.); filtration, extn. into MePh, concn., addn. of Et2O, crystn. (-30°C, 2 d); elem. anal.;
DOI:10.1016/s0020-1693(98)00059-0

Reference yield: 61.0%

: 215254-46-9
(3,5-Me₂C₆H₃N(1-adamantyl))3NbCl

: 917-54-4
methyllithium

: (3,5-Me₂C₆H₃N(1-adamantyl))3Nb(Me)

Guidance literature:: In diethyl ether; byproducts: LiCl; inert atmosphere; stirring Nb-complex with equimolar amt. of LiMe (room temp., 24 h, pptn.); filtration off of LiCl, filtration, concn., crystn. (-30°C), filtration; second crop on evapn. and crystn. from hexane; elem. anal.;
DOI:10.1016/s0020-1693(98)00059-0

Reference yield: 57.0%

: 215254-46-9
(3,5-Me₂C₆H₃N(1-adamantyl))3NbCl

: 591-51-5
phenyllithium

: (3,5-Me₂C₆H₃N(1-adamantyl))3Nb(Ph)

Guidance literature:: In diethyl ether; byproducts: LiCl; inert atmosphere; stirring Nb-complex with 1.5 equiv. of LiPh (room temp., 24 h, pptn.); filtration off of LiCl, evapn., dissoln. in hexane, concn., crystn. (-30°C), filtration; elem. anal.;
DOI:10.1016/s0020-1693(98)00059-0