C₂H₅C₆H₄HgBr

Base Information

• Chemical Name: C₂H₅C₆H₄HgBr
• CAS No.: 156629-29-7
• Molecular Formula: C₈H₉BrHg
• Molecular Weight: 385.653
• Mol file: 156629-29-7.mol

Synonyms:

Chemical Property of C₂H₅C₆H₄HgBr

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₂H₅C₆H₄HgBr

There total 1 articles about C₂H₅C₆H₄HgBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-bromo-4-ethylbenzene (1585-07-5) + mercury dibromide → C2H5C6H4HgBr (156629-29-7)

Guidance literature:

With magnesium; In tetrahydrofuran; addn. of a soln. of HgBr in dry THF to the Grignard reagent (prepared from aryl bromide and Mg in dry THF) under N2, stirring and heating under reflux for 24 h; pouring into cold water, filtn., extn. with CHCl3, evapn. of combined extracts to dryness on a otary evaporator, washing with acetone;

DOI:10.1016/0022-328X(94)80027-8

Reference yield: 60.0%

C2H5C6H4HgBr (156629-29-7) + boron tribromide (10294-33-4) → (4-ethylphenyl)dibromoborane (156629-32-2)

Guidance literature:

In toluene; byproducts: HgBr2; addn. of BBr3 in toluene to a stirred suspn. of arylmercury(II) bromide in toluene under N2, keeping at 90°C for 24 h; cooling to room temp., filtn. to remove HgBr2, removal of solvent under vacuum (room temp./2 mm Hg), distn. of residue in a bulb-to bulb distn. apparatus;

DOI:10.1016/0022-328X(94)80027-8

upstream raw materials:

1-bromo-4-ethylbenzene

Downstream raw materials:

(4-ethylphenyl)dibromoborane