[Me2Pt2(μ-H)(μ-dppm)2](PF6)

Base Information

Chemical Name:[Me2Pt2(μ-H)(μ-dppm)2](PF6)
CAS No.:75862-27-0
Molecular Formula:C₅₂H₅₁P₄Pt₂*F₆P
Molecular Weight:1335
Hs Code.:

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Chemical Property of [Me2Pt2(μ-H)(μ-dppm)2](PF6)

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Technology Process of [Me2Pt2(μ-H)(μ-dppm)2](PF6)

There total 2 articles about [Me2Pt2(μ-H)(μ-dppm)2](PF6) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 17084-13-8
potassium hexafluorophosphate

: 16940-66-2
sodium tetrahydroborate

: 75583-12-9
{Pt₂(CH₃)3((C₆H₅)2PCH₂P(C₆H₅)2)2}⁽¹⁺⁾*PF₆^(1-)={Pt₂(CH₃)3((C₆H₅)2PCH₂P(C₆H₅)2)2}PF₆

: 75862-27-0
[Me2Pt2(μ-H)(μ-dppm)2](PF6)

Guidance literature:: In methanol; Pt complex dissolved in methanol, KPF6 added, cooled to 0°C, NaBH4 in methanol at 0°C added slowly with stirring; ppt. filtered off, recrystd. from CH2Cl2-n-hexane, 2nd crop obtained byfurther crystn. of mother-liquor; elem. anal.;

Reference yield: 77.0%

: 17084-13-8
potassium hexafluorophosphate

: 16940-66-2
sodium tetrahydroborate

: Pt₂Cl(CH₂(P(C₆H₅)2)2)2(CH₃)2⁽¹⁺⁾*PF₆^(1-)=(Pt₂Cl(CH₂(P(C₆H₅)2)2)2(CH₃)2)PF₆

: 75862-27-0
[Me2Pt2(μ-H)(μ-dppm)2](PF6)

Guidance literature:: In methanol; ethanol; water; suspn. of Pt complex in methanol rapidly heated to boiling point, rapidly cooled, NaBH4 in ethanol fairly rapidly added to super-satd. soln., stirred during addn. and then for another 15 min, decanted, treated with aq. KPF6; allowed to ppt. over 1 h, filtered off, washed with water, dried in vac., recrystd. from CH2Cl2-n-hexane; elem. anal.;

Reference yield: 66.0%

: 75862-27-0
[Me2Pt2(μ-H)(μ-dppm)2](PF6)

: 75-05-8,26809-02-9
acetonitrile

: 692-50-2
hexafluoro-2-butyne

: 86802-77-9
[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂CH₃(CF₃CCCF₃)(NCCH₃)]⁽¹⁺⁾*PF₆^(1-)=[((C₆H₅)2PCH₂P(C₆H₅)2)2Pt₂CH₃(CF₃CCCF₃)(NCCH₃)]PF₆

Guidance literature:: In acetonitrile; byproducts: CH4; CF3CCCF3 condensed into tube containing suspn. of Pt complex in MeCN, sealed, allowed to stand at room temp. in dark for 3 d; pptd. by addn. of pentane; elem. anal.;