[(2,5-Dimethyl-3-thienyl)methyl]amine hydrochloride

Base Information

Chemical Name:[(2,5-Dimethyl-3-thienyl)methyl]amine hydrochloride
CAS No.:34843-88-4
Molecular Formula:C₇H₁₁NS
Molecular Weight:141.237
Hs Code.:
Mol file:34843-88-4.mol

Synonyms:

Suppliers and Price of [(2,5-Dimethyl-3-thienyl)methyl]amine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
(2,5-Dimethylthiophen-3-yl)methanamine
2.5g
$ 1232.00

AK Scientific
(2,5-Dimethylthiophen-3-yl)methanamine
250mg
$ 332.00

Total 5 raw suppliers

Chemical Property of [(2,5-Dimethyl-3-thienyl)methyl]amine hydrochloride

Chemical Property:

Boiling Point:100 °C(Press: 12 Torr)
PKA:9.65±0.29(Predicted)
Density:1.074±0.06 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

(2,5-Dimethylthiophen-3-yl)methanamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [(2,5-Dimethyl-3-thienyl)methyl]amine hydrochloride

There total 4 articles about [(2,5-Dimethyl-3-thienyl)methyl]amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26421-26-1
2,5-dimethyl-thiophene-3-carboxylic acid amide

: 34843-88-4
C-(2,5-dimethyl-thiophen-3-yl)-methylamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 4h; Reflux;
DOI:10.1039/c8md00474a

Reference yield:

: 57248-13-2
2,5-dimethylthiophene-3-carbonyl chloride

: 34843-88-4
C-(2,5-dimethyl-thiophen-3-yl)-methylamine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / water; dichloromethane / 1 h / 0 - 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Reflux

With ammonium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c8md00474a

Reference yield:

: 26421-32-9
2,5‐dimethylthiophene‐3‐carboxylic acid

: 34843-88-4
C-(2,5-dimethyl-thiophen-3-yl)-methylamine

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / toluene / 2 h / Reflux

2: ammonium hydroxide / water; dichloromethane / 1 h / 0 - 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Reflux

With ammonium hydroxide; lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1039/c8md00474a