<(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-D-3S-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester

Base Information

• Chemical Name: <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-D-3S-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester
• CAS No.: 138246-03-4
• Molecular Formula: C₅₂H₅₇N₃O₁₁S
• Molecular Weight: 933.096

Synonyms:

Chemical Property of <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-D-3S-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-D-3S-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester

There total 44 articles about <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-D-3S-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

<(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteine (111360-78-2,131478-88-1) + 2R3R/2S3S-2-amino-<3-2H1>pent-4-enoic acid benzhydryl ester (138246-02-3,138246-11-4) → <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-L-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester (138246-03-4,138332-04-4) + <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-D-3R-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester (138246-03-4,138332-04-4)

Guidance literature:

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane; for 24h; Ambient temperature;

DOI:10.1016/S0040-4020(01)91015-4

Reference yield: 42.0%

<(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteine (111360-78-2,131478-88-1) + 2R3R/2S3S-2-amino-<3-2H1>pent-4-enoic acid benzhydryl ester (138246-02-3,138246-11-4) → <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-L-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester (138246-03-4,138332-04-4) + <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-D-3R-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester (138246-03-4,138332-04-4)

Guidance literature:

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane; for 24h; Ambient temperature;

DOI:10.1016/S0040-4020(01)91015-4

Reference yield: 34.0%

<(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteine (111360-78-2,131478-88-1) + 2R3S/2S3R-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester (138246-12-5) → <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-L-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester (138246-03-4,138332-04-4) + <(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteinyl-D-3S-2-amino-<3,4-2H2>pent-4-enoic acid benzhydryl ester (138246-03-4,138332-04-4)

Guidance literature:

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane; for 24h; Ambient temperature;

DOI:10.1016/S0040-4020(01)91015-4

upstream raw materials:

<(N-4-methoxybenzyloxycarbonyl)-(α-4-methoxybenzyl)-δ-(L-α-aminoadipoyl)>-S-(4-methoxybenzyl)-L-cysteine

2R3R/2S3S-2-amino-<3-2H1>pent-4-enoic acid benzhydryl ester

S-(4-methoxybenzyl)-L-cysteine

N-(4-methoxybenzyloxycarbonyl)-α-(4-methoxybenzylester)-δ-L-α-aminoadipic acid

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