cis-5,6-dihydro-1-methylbenzanthracene-5,6-diol

Base Information

• Chemical Name: cis-5,6-dihydro-1-methylbenz
• Molecular Formula: C₁₉H₁₆O₂
• Molecular Weight: 276.335

Synonyms:

Chemical Property of cis-5,6-dihydro-1-methylbenz

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

There total 3 articles about cis-5,6-dihydro-1-methylbenzanthracene-5,6-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1-methylbenz[a]anthracene (2498-77-3) → cis-5,6-dihydro-1-methylbenzanthracene-5,6-diol (87668-39-1,94850-03-0,94850-04-1,107655-83-4,107655-84-5,107656-01-9,107656-02-0)

Guidance literature:

1-methylbenz[a]anthracene; With osmium(VIII) oxide; In pyridine; for 168h; exclusion of light and air;

With sodium hydrogensulfite; In water; for 3h;

DOI:10.1093/mutage/9.2.83

Reference yield:

1-methylbenzanthracene 5,6-oxide (146683-80-9) → cis-5,6-dihydro-1-methylbenzanthracene-5,6-diol (87668-39-1,94850-03-0,94850-04-1,107655-83-4,107655-84-5,107656-01-9,107656-02-0) + 1-Methyl-benzo[a]anthracen-5-ol (133794-66-8) + 1-Methyl-benzo[a]anthracen-6-ol (133794-67-9) + (5S,6S)-1-Methyl-5,6-dihydro-benzo[a]anthracene-5,6-diol (87668-39-1,94850-03-0,94850-04-1,107655-83-4,107655-84-5,107656-01-9,107656-02-0)

Guidance literature:

With water; In 1,4-dioxane; at 25 ℃; Rate constant; Product distribution;

DOI:10.1021/ja00010a036

Reference yield:

1-methylbenzanthracene 5,6-oxide (146683-80-9) → cis-5,6-dihydro-1-methylbenzanthracene-5,6-diol (87668-39-1,94850-03-0,94850-04-1,107655-83-4,107655-84-5,107656-01-9,107656-02-0) + 1-Methyl-benzo[a]anthracen-5-ol (133794-66-8) + 1-Methyl-benzo[a]anthracen-6-ol (133794-67-9) + (5S,6S)-1-Methyl-5,6-dihydro-benzo[a]anthracene-5,6-diol (87668-39-1,94850-03-0,94850-04-1,107655-83-4,107655-84-5,107656-01-9,107656-02-0)

Guidance literature:

With water; In 1,4-dioxane; at 25 ℃; Rate constant; Product distribution;

DOI:10.1021/ja00010a036

upstream raw materials:

1-methylbenz[a]anthracene

1-methylbenzanthracene 5,6-oxide

Downstream raw materials:

3-(2-formyl-6-methyl-phenyl)-naphthalene-2-carbaldehyde

1a,11b-dihydro-5-methyl-1H-benz<3,4>anthra<1,2-b>aziridine

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