D-fucose phenylosazone

Base Information

• Chemical Name: D-fucose phenylosazone
• CAS No.: 6128-23-0
• Molecular Formula: C₁₈H₂₂N₄O₃
• Molecular Weight: 342.398
• Mol file: 6128-23-0.mol

Synonyms:

Chemical Property of D-fucose phenylosazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of D-fucose phenylosazone

There total 3 articles about D-fucose phenylosazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

25(S)-ruscogenin 1-O-β-D-fucopyranosido-3-O-α-L-rhamnopyranoside (87425-34-1) → D-fucose phenylosazone (6128-23-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 2 N HCl-50 percent dioxane / 3 h / Heating

2: AcONa / H₂O / 0.5 h / Heating

With hydrogenchloride; sodium acetate; In water;

Reference yield:

25(S)-ruscogenin 1-O-α-L-rhamnopyranosyl-(1->2)-β-D-fucopyranoside (38971-41-4,87425-35-2) → D-fucose phenylosazone (6128-23-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 2 N HCl-50 percent dioxane / 3 h / Heating

2: AcONa / H₂O / 0.5 h / Heating

With hydrogenchloride; sodium acetate; In water;

Reference yield:

→ D-fucose phenylosazone (6128-23-0)

Guidance literature:

Methyl-2.3-O-isopropyliden-6-desoxy-α-D-talofuranosid, 1) Saeurehydrolyse, 2) Phenylhydrazin;

DOI:10.1021/ja00961a057

upstream raw materials:

25(S)-ruscogenin 1-O-α-L-rhamnopyranosyl-(1->2)-β-D-fucopyranoside

25(S)-ruscogenin 1-O-β-D-fucopyranosido-3-O-α-L-rhamnopyranoside

Refernces