(E)-5-[1-Phenylsulfanyl-meth-(Z)-ylidene]-cyclodecene

Base Information

Chemical Name:(E)-5-[1-Phenylsulfanyl-meth-(Z)-ylidene]-cyclodecene
CAS No.:141520-37-8
Molecular Formula:C₁₇H₂₂S
Molecular Weight:258.428
Hs Code.:

Synonyms:

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Chemical Property of (E)-5-[1-Phenylsulfanyl-meth-(Z)-ylidene]-cyclodecene

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Technology Process of (E)-5-[1-Phenylsulfanyl-meth-(Z)-ylidene]-cyclodecene

There total 14 articles about (E)-5-[1-Phenylsulfanyl-meth-(Z)-ylidene]-cyclodecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141502-85-4
(E)-methyl 6-hydroxymethyl-hepta-2,6-dienoate

: 141520-37-8
(E)-5-[1-Phenylsulfanyl-meth-(Z)-ylidene]-cyclodecene

Guidance literature:: Multi-step reaction with 10 steps

1: 85 percent

2: 95 percent / DIBAL

3: 64 percent / LiBr, MsCl, Et₃N

4: 57 percent / LDA

5: Na-Hg / ethanol

6: n-Bu₃NF

7: n-Bu₃P

8: HCl

9: pyridine

10: LDA, DABCO / tetrahydrofuran

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; hydrogenchloride; sodium amalgam; tributylphosphine; n-Bu₃NF; diisobutylaluminium hydride; methanesulfonyl chloride; triethylamine; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; ethanol;
DOI:10.1246/cl.1992.527

Reference yield:

: 141502-83-2
4-Methoxymethoxymethyl-pent-4-enal

: 141520-37-8
(E)-5-[1-Phenylsulfanyl-meth-(Z)-ylidene]-cyclodecene

Guidance literature:: Multi-step reaction with 12 steps

1: 82 percent / NaH

2: 88 percent / p-TsOH / ethanol

3: 85 percent

4: 95 percent / DIBAL

5: 64 percent / LiBr, MsCl, Et₃N

6: 57 percent / LDA

7: Na-Hg / ethanol

8: n-Bu₃NF

9: n-Bu₃P

10: HCl

11: pyridine

12: LDA, DABCO / tetrahydrofuran

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; hydrogenchloride; sodium amalgam; tributylphosphine; n-Bu₃NF; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; methanesulfonyl chloride; triethylamine; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; ethanol;
DOI:10.1246/cl.1992.527

Reference yield:

: 141502-82-1
4-Methoxymethoxymethyl-pent-4-en-1-ol

: 141520-37-8
(E)-5-[1-Phenylsulfanyl-meth-(Z)-ylidene]-cyclodecene

Guidance literature:: Multi-step reaction with 13 steps

1: 84 percent / (COCl)2, DMSO

2: 82 percent / NaH

3: 88 percent / p-TsOH / ethanol

4: 85 percent

5: 95 percent / DIBAL

6: 64 percent / LiBr, MsCl, Et₃N

7: 57 percent / LDA

8: Na-Hg / ethanol

9: n-Bu₃NF

10: n-Bu₃P

11: HCl

12: pyridine

13: LDA, DABCO / tetrahydrofuran

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; hydrogenchloride; sodium amalgam; oxalyl dichloride; tributylphosphine; n-Bu₃NF; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; ethanol;
DOI:10.1246/cl.1992.527