rengyoxide dimethyl ketal diacetate

Base Information

Chemical Name:rengyoxide dimethyl ketal diacetate
CAS No.:93697-55-3
Molecular Formula:C₁₄H₂₄O₆
Molecular Weight:288.341
Hs Code.:

Synonyms:

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Chemical Property of rengyoxide dimethyl ketal diacetate

Chemical Property:

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Technology Process of rengyoxide dimethyl ketal diacetate

There total 5 articles about rengyoxide dimethyl ketal diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93675-93-5
rengyol monoacetate

: 93697-55-3
rengyoxide dimethyl ketal diacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 39 mg / Collins reagens / CH₂Cl₂ / Ambient temperature

2: 5 percent sodium hydroxide / H₂O; methanol

3: 15 mg / 5 percent hydrogen chloride / Ambient temperature

4: 7 mg / 4-dimethylaminopyridine / triethylamine / Ambient temperature

With hydrogenchloride; dmap; sodium hydroxide; Collins oxidation agent; In methanol; dichloromethane; water; triethylamine;
DOI:10.1139/v84-343

Reference yield:

: 93675-85-5,101489-38-7
rengyol

: 93697-55-3
rengyoxide dimethyl ketal diacetate

Guidance literature:: Multi-step reaction with 5 steps

1: 171 mg / ethanol; pyridine / 48 h / Ambient temperature

2: 39 mg / Collins reagens / CH₂Cl₂ / Ambient temperature

3: 5 percent sodium hydroxide / H₂O; methanol

4: 15 mg / 5 percent hydrogen chloride / Ambient temperature

5: 7 mg / 4-dimethylaminopyridine / triethylamine / Ambient temperature

With hydrogenchloride; dmap; sodium hydroxide; Collins oxidation agent; In pyridine; methanol; ethanol; dichloromethane; water; triethylamine;
DOI:10.1139/v84-343

Reference yield:

: 93675-86-6
rengyoxide

: 93697-55-3
rengyoxide dimethyl ketal diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 15 mg / 5 percent hydrogen chloride / Ambient temperature

2: 7 mg / 4-dimethylaminopyridine / triethylamine / Ambient temperature

With hydrogenchloride; dmap; In triethylamine;
DOI:10.1139/v84-343