Acridine, 9-chloro-3-nitro-5-phenyl-

Base Information

• Chemical Name: Acridine, 9-chloro-3-nitro-5-phenyl-
• CAS No.: 105643-46-7
• Molecular Formula: C₁₉H₁₁ClN₂O₂
• Molecular Weight: 334.762
• Mol file: 105643-46-7.mol

Synonyms:

Chemical Property of Acridine, 9-chloro-3-nitro-5-phenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acridine, 9-chloro-3-nitro-5-phenyl-

There total 3 articles about Acridine, 9-chloro-3-nitro-5-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2-(biphenyl-2-ylamino)-4-nitrobenzoic acid (105643-45-6) → 9-chloro-3-nitro-5-phenylacridine (105643-46-7)

Guidance literature:

With trichlorophosphate; for 3h; Heating;

Reference yield:

2-chloro-4-nitrobenzoic acid (99-60-5) → 9-chloro-3-nitro-5-phenylacridine (105643-46-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) K₂CO₃ / 2.) copper catalyst / 1.) amyl alcohol, 130 deg C, 2.) reflux, 7 h

2: 74 percent / POCl₃ / 3 h / Heating

With potassium carbonate; trichlorophosphate; copper;

Reference yield:

2-phenylaniline (90-41-5) → 9-chloro-3-nitro-5-phenylacridine (105643-46-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) K₂CO₃ / 2.) copper catalyst / 1.) amyl alcohol, 130 deg C, 2.) reflux, 7 h

2: 74 percent / POCl₃ / 3 h / Heating

With potassium carbonate; trichlorophosphate; copper;

upstream raw materials:

2-(biphenyl-2-ylamino)-4-nitrobenzoic acid

2-chloro-4-nitrobenzoic acid

2-phenylaniline

Refernces