4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine

Base Information

Chemical Name:4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine
CAS No.:960379-14-0
Molecular Formula:C₁₉H₂₁N₃OS
Molecular Weight:339.461
Hs Code.:

Synonyms:

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Chemical Property of 4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine

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Technology Process of 4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine

There total 1 articles about 4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84006-10-0
(chloromethyl)-4-methoxy-3,5-dimethylpyridine

: 149739-35-5
3(5)-<2'-methylthiophenyl>pyrazole

: 960379-14-0
4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine

Guidance literature:: With tetra(n-butyl)ammonium hydroxide; sodium hydroxide; In water; toluene; Inert atmosphere;
DOI:10.1021/ja109413c

Reference yield: 90.0%

: tetrakis(acetonitrile)copper(I)tetrafluoroborate

: 960379-14-0
4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine

: 603-35-0
triphenylphosphine

: 960379-11-7
[Cu(4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine)(triphenylphosphine)]BF₄

Guidance literature:: In acetonitrile; (N2); a soln. of Cu complex added to a soln. of ligands at room temp., reacted for 1 h; dried (vac.), recrystd. (CH2Cl2/hexane); elem. anal.;
DOI:10.1021/ic701189b

Reference yield: 70.0%

: 960379-14-0
4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine

: 771-62-0
pentafluorophenylthiol

: copper(l) chloride

: [Cu6(4-methoxy-3,5-dimethyl-2-((3-(2-(methylthio)phenyl)-1H-pyrazol-1-yl)methyl)pyridine)2(pentafluorothiophenolato)6]

Guidance literature:: With NH₃; In water; acetonitrile; (N2); CH3OC5HN(CH3)2CH2C3H2N2C6H4SCH3 added to a suspn. of CuCl, C6F5SH and NH3/H2O added after minutes, reacted for 30 min; H2O added, filtered, dried (vac.); elem. anal.;
DOI:10.1021/ic701189b