Se-Phenyl (5E,9E,13E)-5,9,13-trimethyloctadeca-5,9,13,17-tetraeneselenoate

Base Information

Chemical Name:Se-Phenyl (5E,9E,13E)-5,9,13-trimethyloctadeca-5,9,13,17-tetraeneselenoate
CAS No.:157192-75-1
Molecular Formula:C₂₇H₃₈OSe
Molecular Weight:457.558
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Se-Phenyl (5E,9E,13E)-5,9,13-trimethyloctadeca-5,9,13,17-tetraeneselenoate

Chemical Property:

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Technology Process of Se-Phenyl (5E,9E,13E)-5,9,13-trimethyloctadeca-5,9,13,17-tetraeneselenoate

There total 14 articles about Se-Phenyl (5E,9E,13E)-5,9,13-trimethyloctadeca-5,9,13,17-tetraeneselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1666-13-3
diphenyl diselenide

: 174578-77-9
(5E,9E,13E)-5,9,13-Trimethyl-octadeca-5,9,13,17-tetraenoic acid

: 157192-75-1
Se-Phenyl (5E,9E,13E)-5,9,13-trimethyloctadeca-5,9,13,17-tetraeneselenoate

Guidance literature:: With tributylphosphine;

Reference yield:

: 53268-46-5
3-Hydroxy-2-methylhepta-1,6-diene

: 157192-75-1
Se-Phenyl (5E,9E,13E)-5,9,13-trimethyloctadeca-5,9,13,17-tetraeneselenoate

Guidance literature:: Multi-step reaction with 13 steps

1: EtCO₂H

2: LiAlH₄

3: PCC / CH₂Cl₂

4: 74 percent

5: Hg(OAc)2

6: Heating

7: 58 percent

8: Hg(OAc)2

9: Heating

10: 75 percent / LiN(SiMe₃)2

11: 75 percent / PCC / CH₂Cl₂

12: 73 percent / aq. K₂CO₃ / methanol

13: 73 percent / PBu₃

With lithium aluminium tetrahydride; tributylphosphine; mercury(II) diacetate; potassium carbonate; propionic acid; pyridinium chlorochromate; lithium hexamethyldisilazane; In methanol; dichloromethane;

Reference yield:

: 53359-96-9
Ethyl (4E)-4-methyl-4,8-nonadienoate

: 157192-75-1
Se-Phenyl (5E,9E,13E)-5,9,13-trimethyloctadeca-5,9,13,17-tetraeneselenoate

Guidance literature:: Multi-step reaction with 12 steps

1: LiAlH₄

2: PCC / CH₂Cl₂

3: 74 percent

4: Hg(OAc)2

5: Heating

6: 58 percent

7: Hg(OAc)2

8: Heating

9: 75 percent / LiN(SiMe₃)2

10: 75 percent / PCC / CH₂Cl₂

11: 73 percent / aq. K₂CO₃ / methanol

12: 73 percent / PBu₃

With lithium aluminium tetrahydride; tributylphosphine; mercury(II) diacetate; potassium carbonate; pyridinium chlorochromate; lithium hexamethyldisilazane; In methanol; dichloromethane;