acetic acid 3-{N'-benzyl-N'-[3-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-2-isobutoxycarbonyloxy-4-phenyl-butyryl]-hydrazinocarbonyl}-2-methyl-phenyl ester

Base Information

Chemical Name:acetic acid 3-{N'-benzyl-N'-[3-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-2-isobutoxycarbonyloxy-4-phenyl-butyryl]-hydrazinocarbonyl}-2-methyl-phenyl ester
CAS No.:521275-22-9
Molecular Formula:C₄₁H₅₂N₄O₁₀S
Molecular Weight:792.951
Hs Code.:

acetic acid 3-{<i>N</i>'-benzyl-<i>N</i>'-[3-(2-<i>tert</i>-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-2-isobutoxycarbonyloxy-4-phenyl-butyryl]-hydrazinocarbonyl}-2-methyl-phenyl ester

Synonyms:

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Chemical Property of acetic acid 3-{N'-benzyl-N'-[3-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-2-isobutoxycarbonyloxy-4-phenyl-butyryl]-hydrazinocarbonyl}-2-methyl-phenyl ester

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Technology Process of acetic acid 3-{N'-benzyl-N'-[3-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-2-isobutoxycarbonyloxy-4-phenyl-butyryl]-hydrazinocarbonyl}-2-methyl-phenyl ester

There total 5 articles about acetic acid 3-{N'-benzyl-N'-[3-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-2-isobutoxycarbonyloxy-4-phenyl-butyryl]-hydrazinocarbonyl}-2-methyl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 168899-58-9
3-acetoxy-2-methylbenzoic acid

: 521275-22-9
acetic acid 3-{N'-benzyl-N'-[3-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-2-isobutoxycarbonyloxy-4-phenyl-butyryl]-hydrazinocarbonyl}-2-methyl-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N; BOP / dimethylformamide

2: NMM / dimethylformamide

3: HCl / dioxane

4: Et₃N; BOP / dimethylformamide

With 4-methyl-morpholine; hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00848-X

Reference yield:

: 555-96-4
Benzylhydrazine

: 521275-22-9
acetic acid 3-{N'-benzyl-N'-[3-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-2-isobutoxycarbonyloxy-4-phenyl-butyryl]-hydrazinocarbonyl}-2-methyl-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N; BOP / dimethylformamide

2: NMM / dimethylformamide

3: HCl / dioxane

4: Et₃N; BOP / dimethylformamide

With 4-methyl-morpholine; hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00848-X

Reference yield:

: 521275-18-3
acetic acid 3-(N'-benzyl-hydrazinocarbonyl)-2-methyl-phenyl ester

: 521275-22-9
acetic acid 3-{N'-benzyl-N'-[3-(2-tert-butoxycarbonylamino-3-methylsulfanyl-propionylamino)-2-isobutoxycarbonyloxy-4-phenyl-butyryl]-hydrazinocarbonyl}-2-methyl-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NMM / dimethylformamide

2: HCl / dioxane

3: Et₃N; BOP / dimethylformamide

With 4-methyl-morpholine; hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00848-X