(4-nitrophenyl)methyl mercaptoacetate disulfide

Base Information

Chemical Name:(4-nitrophenyl)methyl mercaptoacetate disulfide
CAS No.:102652-76-6
Molecular Formula:C₁₈H₁₆N₂O₈S₂
Molecular Weight:452.466
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-nitrophenyl)methyl mercaptoacetate disulfide

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Technology Process of (4-nitrophenyl)methyl mercaptoacetate disulfide

There total 2 articles about (4-nitrophenyl)methyl mercaptoacetate disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 102652-76-6
(4-nitrophenyl)methyl mercaptoacetate disulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / conc.H₂SO₄ / toluene / 2 h / Heating

2: 1.) pyridine, SO₂Cl₂ / 1.) CCl₄, 20 min, 2.) CCl₄, 1,2-dichloroethane, 0 deg C, 20 min

With pyridine; sulfuryl dichloride; sulfuric acid; In toluene;
DOI:10.1021/jo00366a010

Reference yield:

: 1074-82-4
potassium phtalimide

: 64832-05-9
(4-nitrophenyl)methyl mercaptoactate

: 102652-76-6
(4-nitrophenyl)methyl mercaptoacetate disulfide

Guidance literature:: With pyridine; sulfuryl dichloride; Yield given. Multistep reaction; 1.) CCl₄, 20 min, 2.) CCl₄, 1,2-dichloroethane, 0 deg C, 20 min;
DOI:10.1021/jo00366a010