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Technology Process of (13RS)-15-norlabd-8(17)-en-14-ol

(13RS)-15-norlabd-8(17)-en-14-ol

Base Information
  • Chemical Name:(13RS)-15-norlabd-8(17)-en-14-ol
  • CAS No.:121944-19-2
  • Molecular Formula:C19H34O
  • Molecular Weight:278.478
  • Hs Code.:
(13RS)-15-norlabd-8<sup>(17)</sup>-en-14-ol

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Technology Process of (13RS)-15-norlabd-8(17)-en-14-ol

There total 1 articles about (13RS)-15-norlabd-8(17)-en-14-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

manool
596-85-0,1438-62-6,29461-42-5,41357-91-9,106631-38-3

manool

(13RS)-15-norlabd-8<sup>(17)</sup>-en-14-ol
121943-79-1,121944-19-2

(13RS)-15-norlabd-8(17)-en-14-ol

Guidance literature:
Multi-step reaction with 6 steps
1: 5 g / t-butyl hydroperoxide, vanadyl acetylacetonate / benzene
2: 4.7 g / LiAlH4 / diethyl ether / 1 h / Heating
3: 3.5 g / sodium periodate / H2O; methanol / Ambient temperature
4: 3.6 g / sodium hydride, trimethylsulfonium iodide / hexane; dimethylsulfoxide; tetrahydrofuran / 1.) 0 deg C, 0.5 h, 2.) RT
5: 0.6 g / boron trifluoride etherate / diethyl ether / 0.08 h / 0 °C
6: 0.5 g / LiAlH4 / diethyl ether / 1 h / Heating
With tert.-butylhydroperoxide; sodium periodate; lithium aluminium tetrahydride; vanadyl acetylacetonate; boron trifluoride diethyl etherate; trimethylsulphonium iodide; sodium hydride; In tetrahydrofuran; methanol; diethyl ether; hexane; water; dimethyl sulfoxide; benzene;
DOI:10.1071/CH9880711
upstream raw materials:

manool

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