Technology Process of C19H13N5
There total 5 articles about C19H13N5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere
1.2: 4 h / -78 °C / Inert atmosphere
2.1: sodium dichromate dihydrate / acetic acid / 5 h / Reflux
3.1: hydrazine; hydrazine hydrochloride / dimethyl sulfoxide
4.1: manganese(IV) oxide / dichloromethane
With
manganese(IV) oxide; n-butyllithium; sodium dichromate dihydrate; hydrazine hydrochloride; hydrazine;
In
tetrahydrofuran; hexane; dichloromethane; acetic acid; dimethyl sulfoxide;
DOI:10.1039/c2dt31288c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium dichromate dihydrate / acetic acid / 5 h / Reflux
2: hydrazine; hydrazine hydrochloride / dimethyl sulfoxide
3: manganese(IV) oxide / dichloromethane
With
manganese(IV) oxide; sodium dichromate dihydrate; hydrazine hydrochloride; hydrazine;
In
dichloromethane; acetic acid; dimethyl sulfoxide;
DOI:10.1039/c2dt31288c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine; hydrazine hydrochloride / dimethyl sulfoxide
2: manganese(IV) oxide / dichloromethane
With
manganese(IV) oxide; hydrazine hydrochloride; hydrazine;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c2dt31288c
