1,1-bis(hydroxymethyl)-2-methylenecyclohexane

Base Information

Chemical Name:1,1-bis(hydroxymethyl)-2-methylenecyclohexane
CAS No.:77192-44-0
Molecular Formula:C₉H₁₆O₂
Molecular Weight:156.225
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-bis(hydroxymethyl)-2-methylenecyclohexane

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Technology Process of 1,1-bis(hydroxymethyl)-2-methylenecyclohexane

There total 2 articles about 1,1-bis(hydroxymethyl)-2-methylenecyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70254-32-9
2-methylenecyclohexanespiro-2'-oxiran

: 77192-44-0
1,1-bis(hydroxymethyl)-2-methylenecyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Fe(CO)5, 2.) cerium(IV) ammonium nitrate / 1.) benzene, irradiated, room temperature, 2.) acetonitrile, -5 deg C

2: 47 percent / lithium aluminium hydride / tetrahydrofuran

With lithium aluminium tetrahydride; iron pentacarbonyl; ammonium cerium(IV) nitrate; In tetrahydrofuran;
DOI:10.1039/P19810000270

Reference yield:

: 2819-48-9
1,2-bis(methylene)cyclohexane

: 77192-44-0
1,1-bis(hydroxymethyl)-2-methylenecyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / peracetic acid, sodium carbonate, sodium acetate / CH₂Cl₂ / 1 h / 0 °C

2: 1.) Fe(CO)5, 2.) cerium(IV) ammonium nitrate / 1.) benzene, irradiated, room temperature, 2.) acetonitrile, -5 deg C

3: 47 percent / lithium aluminium hydride / tetrahydrofuran

With peracetic acid; lithium aluminium tetrahydride; iron pentacarbonyl; ammonium cerium(IV) nitrate; sodium acetate; sodium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/P19810000270