Rh(CO)2I₂^(1-)*P(C₆H₅)4⁽¹⁺⁾={Rh(CO)2I₂}P(C₆H₅)4

Base Information

Chemical Name:Rh(CO)2I₂^(1-)*P(C₆H₅)4⁽¹⁺⁾={Rh(CO)2I₂}P(C₆H₅)4
CAS No.:132099-36-6
Molecular Formula:C₂I₂O₂Rh*C₂₄H₂₀P
Molecular Weight:752.132
Hs Code.:

Rh(CO)2I<sub>2</sub><sup>(1-)</sup>*P(C<sub>6</sub>H<sub>5</sub>)4<sup>(1+)</sup>={Rh(CO)2I<sub>2</sub>}P(C<sub>6</sub>H<sub>5</sub>)4

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Chemical Property of Rh(CO)2I₂^(1-)*P(C₆H₅)4⁽¹⁺⁾={Rh(CO)2I₂}P(C₆H₅)4

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Technology Process of Rh(CO)2I₂^(1-)*P(C₆H₅)4⁽¹⁺⁾={Rh(CO)2I₂}P(C₆H₅)4

There total 1 articles about Rh(CO)2I₂^(1-)*P(C₆H₅)4⁽¹⁺⁾={Rh(CO)2I₂}P(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: [RhI(CO)₂]₂

: 2065-67-0
tetraphenylphosphonium iodide

: 132099-36-6
Rh(CO)2I₂^(1-)*P(C₆H₅)4⁽¹⁺⁾={Rh(CO)2I₂}P(C₆H₅)4

Guidance literature:: In methanol; treating Rh-complex in MeOH with organic salt in MeOH while stirring under CO (1 atm; 20°C); filtration; reducing volume in vac. to pptn.; sealing under CO; crystn. at 0°C; filtration; reducing volume; cooling to -30°C; drying in vac.; elem. anal.;
DOI:10.1016/0022-328X(90)85517-3