erythro-2-quinuclidinyl-4-methylphenylcarbinol

Base Information

Chemical Name:erythro-2-quinuclidinyl-4-methylphenylcarbinol
CAS No.:72265-49-7
Molecular Formula:C₁₅H₂₁NO
Molecular Weight:231.338
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of erythro-2-quinuclidinyl-4-methylphenylcarbinol

Chemical Property:

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Technology Process of erythro-2-quinuclidinyl-4-methylphenylcarbinol

There total 5 articles about erythro-2-quinuclidinyl-4-methylphenylcarbinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 72265-63-5
2-quinuclidinyl 4-methylphenyl ketone

: 72265-49-7,126671-64-5
erythro-2-quinuclidinyl-4-methylphenylcarbinol

Guidance literature:: With diborane; In tetrahydrofuran; for 6h;
DOI:10.1021/jm00176a014

Reference yield:

: 52601-23-7,94160-98-2,52730-01-5
quinuiclidine-2-carboxylic acid hydrochloride

: 72265-49-7,126671-64-5
erythro-2-quinuclidinyl-4-methylphenylcarbinol

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / dimethylformamide / 24 h

2: 2 h / Heating

3: 28 percent / diethyl ether / 30 h / -78 °C

4: 72 percent / diborane / tetrahydrofuran / 6 h

With thionyl chloride; diborane; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jm00176a014

Reference yield:

: 112176-92-8,39926-11-9
(+/-)-ethyl quinuclidine-2-carboxylate

: 72265-49-7,126671-64-5
erythro-2-quinuclidinyl-4-methylphenylcarbinol

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / diethyl ether / 30 h / -78 °C

2: 72 percent / diborane / tetrahydrofuran / 6 h

With diborane; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00176a014