C₁₅H₁₇⁽²⁾HO

Base Information

• Chemical Name: C₁₅H₁₇⁽²⁾HO
• CAS No.: 1332716-50-3
• Molecular Formula: C₁₅H₁₈O
• Molecular Weight: 215.299
• Mol file: 1332716-50-3.mol

Synonyms:

Chemical Property of C₁₅H₁₇⁽²⁾HO

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of C₁₅H₁₇⁽²⁾HO

There total 1 articles about C₁₅H₁₇⁽²⁾HO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-(-)-tert-butyl cis-3-[2H1]-1-phenylprop-2-enyl carbonate (1237787-30-2) + Cyclohexylidene-(2-methoxy-ethyl)-amine (13652-41-0) → C15H17(2)HO + C15H17(2)HO + C15H17(2)HO + C15H17(2)HO (1332716-50-3) + C15H17(2)HO (1332716-49-0)

Guidance literature:

Cyclohexylidene-(2-methoxy-ethyl)-amine; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

(S)-(-)-tert-butyl cis-3-[2H₁]-1-phenylprop-2-enyl carbonate; With bis(η3-allyl-μ-chloropalladium(II)); P(p-CH₃OC₆H₄)3; In tetrahydrofuran; at 20 ℃; optical yield given as %ee; regioselective reaction; Further stages; Inert atmosphere;

DOI:10.1021/ja2039503

upstream raw materials:

(S)-(-)-tert-butyl cis-3-[2H₁]-1-phenylprop-2-enyl carbonate

Cyclohexylidene-(2-methoxy-ethyl)-amine