decacarbonyl-μ-1-fluoro-1,2-diphenyldiphosphinedichromium

Base Information

Chemical Name:decacarbonyl-μ-1-fluoro-1,2-diphenyldiphosphinedichromium
CAS No.:152748-61-3
Molecular Formula:C₂₂H₁₁Cr₂FO₁₀P₂
Molecular Weight:620.261
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of decacarbonyl-μ-1-fluoro-1,2-diphenyldiphosphinedichromium

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Technology Process of decacarbonyl-μ-1-fluoro-1,2-diphenyldiphosphinedichromium

There total 1 articles about decacarbonyl-μ-1-fluoro-1,2-diphenyldiphosphinedichromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 149951-10-0,97913-00-3
decacarbonyl-μ-1-chloro-1,2-diphenyldiphosphinedichromium

: 429-41-4
tetrabutyl ammonium fluoride

: 152748-61-3,152748-62-4
decacarbonyl-μ-1-fluoro-1,2-diphenyldiphosphinedichromium

Guidance literature:: In toluene; nitrogen; soln. of Cr-complex was added dropwise with stirring to suspension of Bu4NF (toluene) at room temperature; stirred for 45 min; solvent removed at room temperature (vacuo); addn. of diethyl ether; filtration; drying (vacuo); chromatography (silica gel; toluene); eluate was concentrated and kept at -4°C; elem. anal.;
DOI:10.1016/0022-328X(93)80328-9