C₃₇H₅₉BrN₂O₈S

Base Information

Chemical Name:C₃₇H₅₉BrN₂O₈S
CAS No.:1437119-16-8
Molecular Formula:C₃₇H₅₉BrN₂O₈S
Molecular Weight:771.854
Hs Code.:

C<sub>37</sub>H<sub>59</sub>BrN<sub>2</sub>O<sub>8</sub>S

Synonyms:

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Chemical Property of C₃₇H₅₉BrN₂O₈S

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Technology Process of C₃₇H₅₉BrN₂O₈S

There total 18 articles about C₃₇H₅₉BrN₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1437119-11-3
C₃₀H₅₁BrO₇

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1437119-16-8
C₃₇H₅₉BrN₂O₈S

Guidance literature:: In methanol; at 45 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.041

Reference yield:

: C₂₁H₃₄O₅

: 1437119-16-8
C₃₇H₅₉BrN₂O₈S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydrogencarbonate; ozone; oxygen / dichloromethane; methanol / -78 °C / Inert atmosphere

2.1: Schwartz's reagent / dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Darkness

2.2: 0.33 h / -78 °C / Inert atmosphere; Darkness

2.3: -78 - 20 °C / Inert atmosphere; Darkness

3.1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 20 °C / 760.05 Torr / Inert atmosphere

4.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

5.1: methyllithium / tetrahydrofuran; diethyl ether / 2.5 h / -78 °C / Inert atmosphere

6.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0 - 20 °C / Molecular sieve; Inert atmosphere

7.1: methanol / 45 °C / Inert atmosphere

With Schwartz's reagent; tetrapropylammonium perruthennate; palladium 10% on activated carbon; methyllithium; hydrogen; oxygen; sodium hydrogencarbonate; ozone; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane;
DOI:10.1016/j.tet.2013.04.041

Reference yield:

: 106-25-2
Nerol

: 1437119-16-8
C₃₇H₅₉BrN₂O₈S

Guidance literature:: Multi-step reaction with 13 steps

1.1: diethyl (2R,3R)-tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / 3.82 h / Inert atmosphere; Molecular sieve

2.1: 1-methyl-1H-imidazole / toluene / 0 - 20 °C / Inert atmosphere

3.1: Br(coll)2BF₄ / nitromethane / 0.25 h / Inert atmosphere; Cooling with ice

4.1: sodium hydroxide / methanol / 2 h / 20 °C / Inert atmosphere

5.1: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 8 h / 0 - 20 °C / Inert atmosphere

6.1: potassium carbonate / methanol / 16 h / 20 °C / Inert atmosphere

7.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

8.1: Schwartz's reagent / dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Darkness

8.2: 0.33 h / -78 °C / Inert atmosphere; Darkness

8.3: -78 - 20 °C / Inert atmosphere; Darkness

9.1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 20 °C / 760.05 Torr / Inert atmosphere

10.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

11.1: methyllithium / tetrahydrofuran; diethyl ether / 2.5 h / -78 °C / Inert atmosphere

12.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0 - 20 °C / Molecular sieve; Inert atmosphere

13.1: methanol / 45 °C / Inert atmosphere

With 1-methyl-1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; Schwartz's reagent; tetrapropylammonium perruthennate; diethyl (2R,3R)-tartrate; palladium 10% on activated carbon; methyllithium; hydrogen; sulfur trioxide pyridine complex; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; decane; nitromethane; ethanol; dichloromethane; dimethyl sulfoxide; toluene; 6.1: |Seyferth-Gilbert Homologation;
DOI:10.1016/j.tet.2013.04.041