palladium chloride N-(3,5-bis[(diphenylphosphanyl)methyl]phenyl)acetamide

Base Information

Chemical Name:palladium chloride N-(3,5-bis[(diphenylphosphanyl)methyl]phenyl)acetamide
CAS No.:864766-33-6
Molecular Formula:C₃₄H₃₀ClNOP₂Pd
Molecular Weight:672.439
Hs Code.:

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Chemical Property of palladium chloride N-(3,5-bis[(diphenylphosphanyl)methyl]phenyl)acetamide

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Technology Process of palladium chloride N-(3,5-bis[(diphenylphosphanyl)methyl]phenyl)acetamide

There total 1 articles about palladium chloride N-(3,5-bis[(diphenylphosphanyl)methyl]phenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 15475-27-1,4346-39-8
potassium diphenylphosphine

: 251912-30-8
N-acetyl-3,5-bis(chloromethyl)aniline

: 864766-33-6
palladium chloride N-(3,5-bis[(diphenylphosphanyl)methyl]phenyl)acetamide

Guidance literature:: With silver tetrafluoroborate; In dichloromethane; acetonitrile; under N2 atm. KPPh2 in THF was added to soln. CH3CONHC6H3(CH2Cl)2 in THF, refluxed for 3 h, cooled to room temp., solvent was removed in vacuo, dissolved in CH2Cl2, washed with water, evapd., dissolved in CH2Cl2-MeCN, PdCl2(NCPh)2 was added, 30 min; AgBF4 was added and stirred for 30 min, diluted with CH2Cl2, poured intosaturated brine and stirred for 5 h, org. layer was dried over Na2SO4, filtered through silica, evapd., recrystd. from CH2Cl2-Et2O; elem. anal.;
DOI:10.1021/om048992v